Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
A spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 4...
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College of Education for Pure Sciences
2005-06-01
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doaj-46680637e58b4644b0d49ef471de3cd22020-11-25T00:26:47ZaraCollege of Education for Pure Sciencesمجلة التربية والعلم1812-125X2664-25302005-06-01172324010.33899/edusj.2005.8130881308Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation ReactionN. OthmanA spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 420 nm. Beer's law is obeyed over the concentrations range of 0.4-14 ppm. The relative error is -2.47 to + 3.41 % and the relative standard deviation is ±0.51 to ±2.9% depending on the concentration level. The proposed method has been successfully applied to the determination of sulphacetamide sodium in eye drop drug.https://edusj.mosuljournals.com/article_81308_83347e4b5c8eba10a78247e4bda441d7.pdfspectrophotometricpyrogallolsulphacetamide |
collection |
DOAJ |
language |
Arabic |
format |
Article |
sources |
DOAJ |
author |
N. Othman |
spellingShingle |
N. Othman Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction مجلة التربية والعلم spectrophotometric pyrogallol sulphacetamide |
author_facet |
N. Othman |
author_sort |
N. Othman |
title |
Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction |
title_short |
Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction |
title_full |
Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction |
title_fullStr |
Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction |
title_full_unstemmed |
Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction |
title_sort |
spectrophotometic determination of some sulphonamides in aqueous solution via azo- dye formation reaction |
publisher |
College of Education for Pure Sciences |
series |
مجلة التربية والعلم |
issn |
1812-125X 2664-2530 |
publishDate |
2005-06-01 |
description |
A spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 420 nm. Beer's law is obeyed over the concentrations range of 0.4-14 ppm. The relative error is -2.47 to + 3.41 % and the relative standard deviation is ±0.51 to ±2.9% depending on the concentration level. The proposed method has been successfully applied to the determination of sulphacetamide sodium in eye drop drug. |
topic |
spectrophotometric pyrogallol sulphacetamide |
url |
https://edusj.mosuljournals.com/article_81308_83347e4b5c8eba10a78247e4bda441d7.pdf |
work_keys_str_mv |
AT nothman spectrophotometicdeterminationofsomesulphonamidesinaqueoussolutionviaazodyeformationreaction |
_version_ |
1725342599804354560 |