Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction

A spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 4...

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Main Author: N. Othman
Format: Article
Language:Arabic
Published: College of Education for Pure Sciences 2005-06-01
Series:مجلة التربية والعلم
Subjects:
Online Access:https://edusj.mosuljournals.com/article_81308_83347e4b5c8eba10a78247e4bda441d7.pdf
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spelling doaj-46680637e58b4644b0d49ef471de3cd22020-11-25T00:26:47ZaraCollege of Education for Pure Sciencesمجلة التربية والعلم1812-125X2664-25302005-06-01172324010.33899/edusj.2005.8130881308Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation ReactionN. OthmanA spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 420 nm. Beer's law is obeyed over the concentrations range of 0.4-14 ppm. The relative error is -2.47 to + 3.41 % and the relative standard deviation is ±0.51 to ±2.9% depending on the concentration level. The proposed method has been successfully applied to the determination of sulphacetamide sodium in eye drop drug.https://edusj.mosuljournals.com/article_81308_83347e4b5c8eba10a78247e4bda441d7.pdfspectrophotometricpyrogallolsulphacetamide
collection DOAJ
language Arabic
format Article
sources DOAJ
author N. Othman
spellingShingle N. Othman
Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
مجلة التربية والعلم
spectrophotometric
pyrogallol
sulphacetamide
author_facet N. Othman
author_sort N. Othman
title Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
title_short Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
title_full Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
title_fullStr Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
title_full_unstemmed Spectrophotometic Determination of some Sulphonamides in Aqueous Solution Via Azo- Dye Formation Reaction
title_sort spectrophotometic determination of some sulphonamides in aqueous solution via azo- dye formation reaction
publisher College of Education for Pure Sciences
series مجلة التربية والعلم
issn 1812-125X
2664-2530
publishDate 2005-06-01
description A spectrophotometric method for the determination of trace amounts of some sulphonmides (six compounds) in aqueous solutions is described. The method in based on dizotisation and coupling with pyrogallol to form a yellow coloured, stable and water- soluble azo-dye which shows maximum absorption at 420 nm. Beer's law is obeyed over the concentrations range of 0.4-14 ppm. The relative error is -2.47 to + 3.41 % and the relative standard deviation is ±0.51 to ±2.9% depending on the concentration level. The proposed method has been successfully applied to the determination of sulphacetamide sodium in eye drop drug.
topic spectrophotometric
pyrogallol
sulphacetamide
url https://edusj.mosuljournals.com/article_81308_83347e4b5c8eba10a78247e4bda441d7.pdf
work_keys_str_mv AT nothman spectrophotometicdeterminationofsomesulphonamidesinaqueoussolutionviaazodyeformationreaction
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