Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate

Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate

The title compound, C24H30O8, was obtained by reaction of ethyl 4-hydroxybenzoate with 1,2-dichloroethane. The molecule occupies a crystallographic inversion center, with its central ethylene bridge in an anti conformation. The other ethylene bridge has a gauche conformation, with the corresponding...

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Main Authors: Jingjie Fan, Gang Lai, Zhen Ma, Haisha Qin
Format: Article
Language:English
Published: International Union of Crystallography 2012-03-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812004874
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spelling doaj-40d55dfa26ac46d88beda419e63331cd2020-11-25T01:37:49ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-03-01683o714o71410.1107/S1600536812004874Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoateJingjie FanGang LaiZhen MaHaisha QinThe title compound, C24H30O8, was obtained by reaction of ethyl 4-hydroxybenzoate with 1,2-dichloroethane. The molecule occupies a crystallographic inversion center, with its central ethylene bridge in an anti conformation. The other ethylene bridge has a gauche conformation, with the corresponding O—C—C—O torsion angle being 74.2 (1)°. The benzene rings are almost coplanar with the adjacent ethoxycarbonyl groups, with an r.m.s. deviation of 0.078 Å.http://scripts.iucr.org/cgi-bin/paper?S1600536812004874
collection DOAJ
language English
format Article
sources DOAJ
author Jingjie Fan
Gang Lai
Zhen Ma
Haisha Qin
spellingShingle Jingjie Fan
Gang Lai
Zhen Ma
Haisha Qin
Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
Acta Crystallographica Section E
author_facet Jingjie Fan
Gang Lai
Zhen Ma
Haisha Qin
author_sort Jingjie Fan
title Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
title_short Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
title_full Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
title_fullStr Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
title_full_unstemmed Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
title_sort diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-03-01
description The title compound, C24H30O8, was obtained by reaction of ethyl 4-hydroxybenzoate with 1,2-dichloroethane. The molecule occupies a crystallographic inversion center, with its central ethylene bridge in an anti conformation. The other ethylene bridge has a gauche conformation, with the corresponding O—C—C—O torsion angle being 74.2 (1)°. The benzene rings are almost coplanar with the adjacent ethoxycarbonyl groups, with an r.m.s. deviation of 0.078 Å.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812004874
work_keys_str_mv AT jingjiefan diethyl44amp824236dioxaoctane18diyldioxydibenzoate
AT ganglai diethyl44amp824236dioxaoctane18diyldioxydibenzoate
AT zhenma diethyl44amp824236dioxaoctane18diyldioxydibenzoate
AT haishaqin diethyl44amp824236dioxaoctane18diyldioxydibenzoate
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