Synthesis and reduction of 10-phthalimidocamphor oxime

10-Phthalimidocamphor oxime was prepared from easily available 10-iodocamphor in two steps. Reduction of the oxime functionality resulted in the formation of two novel polycyclic isoindolinone heterocycles, the attempted preparation of the primary amine failed. The structures of novel heterocycles w...

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Main Authors: Uroš Grošelj, Amalija Golobič, Jurij Svete, Sebastijan Ričko
Format: Article
Language:English
Published: Slovenian Chemical Society 2017-12-01
Series:Acta Chimica Slovenica
Subjects:
Online Access:https://journals.matheo.si/index.php/ACSi/article/view/3474
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spelling doaj-40069bdc73ec433fb56622e57085f2cb2020-11-25T00:50:00ZengSlovenian Chemical SocietyActa Chimica Slovenica1318-02071580-31552017-12-0164479079710.17344/acsi.2017.3474513Synthesis and reduction of 10-phthalimidocamphor oximeUroš Grošelj0Amalija Golobič1Jurij Svete2Sebastijan Ričko3University of Ljubljana Faculty of Chemistry and Chemical Technology Chair of Organic ChemistryUniversity of Ljubljana Faculty of Chemistry and Chemical Technology Chair of Inorganic ChemistryUniversity of Ljubljana Faculty of Chemistry and Chemical Technology Chair of Organic ChemistryUniversity of Ljubljana Faculty of Chemistry and Chemical Technology Chair of Organic Chemistry10-Phthalimidocamphor oxime was prepared from easily available 10-iodocamphor in two steps. Reduction of the oxime functionality resulted in the formation of two novel polycyclic isoindolinone heterocycles, the attempted preparation of the primary amine failed. The structures of novel heterocycles were unambiguously confirmed by single crystal X-ray diffraction as well as NMR techniques.https://journals.matheo.si/index.php/ACSi/article/view/347410-iodocamphor10-phthalimidocamphor oximecamphor derived aminesreduction
collection DOAJ
language English
format Article
sources DOAJ
author Uroš Grošelj
Amalija Golobič
Jurij Svete
Sebastijan Ričko
spellingShingle Uroš Grošelj
Amalija Golobič
Jurij Svete
Sebastijan Ričko
Synthesis and reduction of 10-phthalimidocamphor oxime
Acta Chimica Slovenica
10-iodocamphor
10-phthalimidocamphor oxime
camphor derived amines
reduction
author_facet Uroš Grošelj
Amalija Golobič
Jurij Svete
Sebastijan Ričko
author_sort Uroš Grošelj
title Synthesis and reduction of 10-phthalimidocamphor oxime
title_short Synthesis and reduction of 10-phthalimidocamphor oxime
title_full Synthesis and reduction of 10-phthalimidocamphor oxime
title_fullStr Synthesis and reduction of 10-phthalimidocamphor oxime
title_full_unstemmed Synthesis and reduction of 10-phthalimidocamphor oxime
title_sort synthesis and reduction of 10-phthalimidocamphor oxime
publisher Slovenian Chemical Society
series Acta Chimica Slovenica
issn 1318-0207
1580-3155
publishDate 2017-12-01
description 10-Phthalimidocamphor oxime was prepared from easily available 10-iodocamphor in two steps. Reduction of the oxime functionality resulted in the formation of two novel polycyclic isoindolinone heterocycles, the attempted preparation of the primary amine failed. The structures of novel heterocycles were unambiguously confirmed by single crystal X-ray diffraction as well as NMR techniques.
topic 10-iodocamphor
10-phthalimidocamphor oxime
camphor derived amines
reduction
url https://journals.matheo.si/index.php/ACSi/article/view/3474
work_keys_str_mv AT urosgroselj synthesisandreductionof10phthalimidocamphoroxime
AT amalijagolobic synthesisandreductionof10phthalimidocamphoroxime
AT jurijsvete synthesisandreductionof10phthalimidocamphoroxime
AT sebastijanricko synthesisandreductionof10phthalimidocamphoroxime
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