Synthesis and reduction of 10-phthalimidocamphor oxime

10-Phthalimidocamphor oxime was prepared from easily available 10-iodocamphor in two steps. Reduction of the oxime functionality resulted in the formation of two novel polycyclic isoindolinone heterocycles, the attempted preparation of the primary amine failed. The structures of novel heterocycles w...

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Bibliographic Details
Main Authors: Uroš Grošelj, Amalija Golobič, Jurij Svete, Sebastijan Ričko
Format: Article
Language:English
Published: Slovenian Chemical Society 2017-12-01
Series:Acta Chimica Slovenica
Subjects:
Online Access:https://journals.matheo.si/index.php/ACSi/article/view/3474
Description
Summary:10-Phthalimidocamphor oxime was prepared from easily available 10-iodocamphor in two steps. Reduction of the oxime functionality resulted in the formation of two novel polycyclic isoindolinone heterocycles, the attempted preparation of the primary amine failed. The structures of novel heterocycles were unambiguously confirmed by single crystal X-ray diffraction as well as NMR techniques.
ISSN:1318-0207
1580-3155