3-[2-(9H-Carbazol-9-yl)ethyl]-4-phenyl-1H-1,2,4-triazole-5(4H)-thione dimethyl sulfoxide monosolvate

In the title compound, C22H18N4S·C2H6OS, the central triazolethione ring is inclined to the carbazole ring system by 13.97 (18)° and to the phenyl ring by 66.4 (1)°. The lattice solvent, dimethyl sulfoxide, is strongly hydrogen bonded to the triazolethione ring. In the crystal, the main molecules fo...

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Bibliographic Details
Main Authors: Shaaban K. Mohamed, Joel T. Mague, Mehmet Akkurt, Talaat I. El-Emary, Mustafa R. Albayati
Format: Article
Language:English
Published: International Union of Crystallography 2016-11-01
Series:IUCrData
Subjects:
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2414314616018356
Description
Summary:In the title compound, C22H18N4S·C2H6OS, the central triazolethione ring is inclined to the carbazole ring system by 13.97 (18)° and to the phenyl ring by 66.4 (1)°. The lattice solvent, dimethyl sulfoxide, is strongly hydrogen bonded to the triazolethione ring. In the crystal, the main molecules form columns parallel to the a axis, with the solvent molecules located between the columns. C—H...S hydrogen bonds and C—H...π(ring) interactions link adjacent columns. The crystal studied was refined as a two-component twin, with a fractional contribution to the minor domain of 0.0742 (14).
ISSN:2414-3146