3-[2-(9H-Carbazol-9-yl)ethyl]-4-phenyl-1H-1,2,4-triazole-5(4H)-thione dimethyl sulfoxide monosolvate
In the title compound, C22H18N4S·C2H6OS, the central triazolethione ring is inclined to the carbazole ring system by 13.97 (18)° and to the phenyl ring by 66.4 (1)°. The lattice solvent, dimethyl sulfoxide, is strongly hydrogen bonded to the triazolethione ring. In the crystal, the main molecules fo...
Main Authors: | , , , , |
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Format: | Article |
Language: | English |
Published: |
International Union of Crystallography
2016-11-01
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Series: | IUCrData |
Subjects: | |
Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314616018356 |
Summary: | In the title compound, C22H18N4S·C2H6OS, the central triazolethione ring is inclined to the carbazole ring system by 13.97 (18)° and to the phenyl ring by 66.4 (1)°. The lattice solvent, dimethyl sulfoxide, is strongly hydrogen bonded to the triazolethione ring. In the crystal, the main molecules form columns parallel to the a axis, with the solvent molecules located between the columns. C—H...S hydrogen bonds and C—H...π(ring) interactions link adjacent columns. The crystal studied was refined as a two-component twin, with a fractional contribution to the minor domain of 0.0742 (14). |
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ISSN: | 2414-3146 |