Quasi-Static Shear Test of Hybrid Adhesive Bonds Based on Treated Cotton-Epoxy Resin Layer

• Main Authors: Martin Tichý, Viktor Kolář, Miroslav Müller, Rajesh Kumar Mishra, Vladimír Šleger, Monika Hromasová
• Format: Article
• Language: English
• Published: MDPI AG 2020-12-01
• Series: Polymers
• Subjects: mechanical behavior; fatigue and fracture mechanics; green composite; biological fabric; alkali treatment; SEM analyses
• Online Access: https://www.mdpi.com/2073-4360/12/12/2945

This research evaluates the mechanical properties of hybrid adhesive bonds with various 100% cotton fabrics in static and quasi-static conditions and the influence of alkali surface treatment (NaOH) of the cotton fabrics on the mechanical properties. Biological fibers in polymers are characterized by low wettability with the matrix, which decreases mechanical properties. Adhesive bonds usually operate in cyclic stress, which causes irreversible failure before maximal strength. In this paper, a quasi-static test was used to load the adhesive bonds in 5–50% (192–1951 N) and 5–70% (192–2732 N) intervals with 1000 cycles. The results of SEM analysis showed good wettability of alkali treated cotton fabric with NaOH solution in hybrid adhesive bonds. The static test proved the influence of reinforcing cotton fabrics on shear tensile strength against pure resin, i.e., sample Erik up to 19% on 14.90 ± 1.15 MPa and sample Tera up to 21% on 15.28 ± 1.05 MPa. The adhesive bonds with pure resin did not resist either quasi-static tests. Reinforcing cotton fabrics resisted both quasi-static tests, even shear tensile strength increases up to 10% on 16.34 ± 1.24 MPa for the fabric Erik. The results of strain difference of adhesive bonds with Tera and Erik confirmed that a lower value of the difference during cyclic loading positively influenced the ultimate shear tensile strength.