Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography

Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography

The composition of multicomponent determination by colorimetric titration is difficult. This complexity is easily overcome by using Gas Chromatography technique instead of wet method for multi-component mixture analysis. In Gas Chromatography, first the standard chart is prepared by using the known...

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Main Authors: Mallaiah Mekala, Venkat Reddy Goli
Format: Article
Language:English
Published: Elsevier 2018-06-01
Series:Data in Brief
Online Access:http://www.sciencedirect.com/science/article/pii/S235234091830324X
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spelling doaj-3b4c9eef62334dcb9be3b26f682071d52020-11-25T01:33:50ZengElsevierData in Brief2352-34092018-06-0118947960Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas ChromatographyMallaiah Mekala0Venkat Reddy Goli1Department of Chemical Engineering, BV Raju Institute of Technology, Hyderabad 502313, India; Corresponding author.Department of Chemical Engineering, National Institute of Technology, Warangal 506004, IndiaThe composition of multicomponent determination by colorimetric titration is difficult. This complexity is easily overcome by using Gas Chromatography technique instead of wet method for multi-component mixture analysis. In Gas Chromatography, first the standard chart is prepared by using the known amount sample concentration as the reference. Once calibration chart is prepared the unknown sample concentration easily measured by using the standard chart. In the present study a standard calibration chart developed for the four component system of acetic acid–methanol–methyl acetate–water. The samples were taken at various concentrations of all components and different chromatograms obtained under various concentrations respectively. The method of optimization was first carried out to get the sharp peaks of individual components and binary pairs also. By using those conditions, the multi components concentrations were estimated. From the present results, the area under gas chromatogram is linearly varying with mole% of the components compared to mass%. Keywords: Gas Chromatography, Esterification, Calibration, Retention time, Optimizationhttp://www.sciencedirect.com/science/article/pii/S235234091830324X
collection DOAJ
language English
format Article
sources DOAJ
author Mallaiah Mekala
Venkat Reddy Goli
spellingShingle Mallaiah Mekala
Venkat Reddy Goli
Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography
Data in Brief
author_facet Mallaiah Mekala
Venkat Reddy Goli
author_sort Mallaiah Mekala
title Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography
title_short Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography
title_full Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography
title_fullStr Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography
title_full_unstemmed Data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column Gas Chromatography
title_sort data on acetic acid–methanol–methyl acetate–water mixture analysised by dual packed column gas chromatography
publisher Elsevier
series Data in Brief
issn 2352-3409
publishDate 2018-06-01
description The composition of multicomponent determination by colorimetric titration is difficult. This complexity is easily overcome by using Gas Chromatography technique instead of wet method for multi-component mixture analysis. In Gas Chromatography, first the standard chart is prepared by using the known amount sample concentration as the reference. Once calibration chart is prepared the unknown sample concentration easily measured by using the standard chart. In the present study a standard calibration chart developed for the four component system of acetic acid–methanol–methyl acetate–water. The samples were taken at various concentrations of all components and different chromatograms obtained under various concentrations respectively. The method of optimization was first carried out to get the sharp peaks of individual components and binary pairs also. By using those conditions, the multi components concentrations were estimated. From the present results, the area under gas chromatogram is linearly varying with mole% of the components compared to mass%. Keywords: Gas Chromatography, Esterification, Calibration, Retention time, Optimization
url http://www.sciencedirect.com/science/article/pii/S235234091830324X
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AT venkatreddygoli dataonaceticacidmethanolmethylacetatewatermixtureanalysisedbydualpackedcolumngaschromatography
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