Novel Characterization Techniques for Additive Manufacturing Powder Feedstock

• Main Authors: Benjamin Young, Joseph Heelan, Sean Langan, Matthew Siopis, Caitlin Walde, Aaron Birt
• Format: Article
• Language: English
• Published: MDPI AG 2021-04-01
• Series: Metals
• Subjects: additive manufacturing; metal powders; cermet powders; characterization; cold spray
• Online Access: https://www.mdpi.com/2075-4701/11/5/720

Additive manufacturing is a rapidly expanding field, encompassing many methods to manufacture parts and coatings with a wide variety of feedstock. Metal powders are one such feedstock, with a range of compositions and morphologies. Understanding subtle changes in the feedstock is critical to ensure successful consolidation and quality control of both the feedstock and manufactured part. Current standards lack the ability to finely distinguish almost acceptable powders from barely acceptable ones. Here, novel means of powder feedstock characterization for quality control are demonstrated for the solid-state AM process of cold spray, though similar methods may be extrapolated to other additive methods as well. These characterization methods aim to capture the physics of the process, which in cold spray consists of high strain rate deformation of solid-state feedstock. To capture this, in this effort powder compaction was evaluated via rapidly applied loads, flowability of otherwise non-flowable powders was evaluated with the addition of vibration, and powder electrical resistivity was evaluated through compaction between two electrodes. Several powders, including aluminum alloys, chromium, and cermet composites, were evaluated in this effort, with each case study demonstrating the need for non-traditional characterization metrics as a means of quality control and classification of these materials.