Preparation of TiO2 anatase nanocrystals by TiCl4 hydrolysis with additive H2SO4.

A new methodology was developed to synthesize uniform titania anatase nanocrystals by the hydrolysis of titanium chloride in sulfuric acid aqueous solutions at 0-90°C. The samples were characterized by Raman spectroscopy, UV-visible spectroscopy, transmission electron microscopy (TEM), electron diff...

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Bibliographic Details
Main Authors: Wenbing Li, Tingying Zeng
Format: Article
Language:English
Published: Public Library of Science (PLoS) 2011-01-01
Series:PLoS ONE
Online Access:http://europepmc.org/articles/PMC3115985?pdf=render