1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate

1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate

The asymmetric unit of the title solvate, C20H14O4·2C2D6OS, contains half of the substituted terephthalic acid molecule and one solvent molecule. The centroid of the central benzene ring in the acid molecule is coincident with a crystallographic inversion center. Neither the carboxyl no...

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Bibliographic Details
Main Authors: Lucian C. Pop, Marcelo Preite, Juan Manuel Manriquez, Andrés Vega, Ivonne Chavez
Format: Article
Language:English
Published: International Union of Crystallography 2012-04-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812012056
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spelling doaj-3779d4c1b13f4541a9e21030721b6a4a2020-11-24T21:26:28ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-04-01684o1192o119210.1107/S16005368120120561,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvateLucian C. PopMarcelo PreiteJuan Manuel ManriquezAndrés VegaIvonne ChavezThe asymmetric unit of the title solvate, C20H14O4·2C2D6OS, contains half of the substituted terephthalic acid molecule and one solvent molecule. The centroid of the central benzene ring in the acid molecule is coincident with a crystallographic inversion center. Neither the carboxyl nor the phenyl substituents are coplanar with the central aromatic ring, showing dihedral angles of 53.18 (11) and 47.83 (11)°, respectively. The dimethyl sulfoxide solvent molecules are hydrogen bonded to the carboxylic acid groups.http://scripts.iucr.org/cgi-bin/paper?S1600536812012056
collection DOAJ
language English
format Article
sources DOAJ
author Lucian C. Pop
Marcelo Preite
Juan Manuel Manriquez
Andrés Vega
Ivonne Chavez
spellingShingle Lucian C. Pop
Marcelo Preite
Juan Manuel Manriquez
Andrés Vega
Ivonne Chavez
1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
Acta Crystallographica Section E
author_facet Lucian C. Pop
Marcelo Preite
Juan Manuel Manriquez
Andrés Vega
Ivonne Chavez
author_sort Lucian C. Pop
title 1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
title_short 1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
title_full 1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
title_fullStr 1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
title_full_unstemmed 1,1′:4′,1′′-Terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
title_sort 1,1′:4′,1′′-terphenyl-2′,5′-dicarboxylic acid dimethyl sulfoxide-d6 disolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-04-01
description The asymmetric unit of the title solvate, C20H14O4·2C2D6OS, contains half of the substituted terephthalic acid molecule and one solvent molecule. The centroid of the central benzene ring in the acid molecule is coincident with a crystallographic inversion center. Neither the carboxyl nor the phenyl substituents are coplanar with the central aromatic ring, showing dihedral angles of 53.18 (11) and 47.83 (11)°, respectively. The dimethyl sulfoxide solvent molecules are hydrogen bonded to the carboxylic acid groups.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812012056
work_keys_str_mv AT luciancpop 11amp82424amp82421amp8242amp8242terphenyl2amp82425amp8242dicarboxylicaciddimethylsulfoxided6disolvate
AT marcelopreite 11amp82424amp82421amp8242amp8242terphenyl2amp82425amp8242dicarboxylicaciddimethylsulfoxided6disolvate
AT juanmanuelmanriquez 11amp82424amp82421amp8242amp8242terphenyl2amp82425amp8242dicarboxylicaciddimethylsulfoxided6disolvate
AT andramp233svega 11amp82424amp82421amp8242amp8242terphenyl2amp82425amp8242dicarboxylicaciddimethylsulfoxided6disolvate
AT ivonnechavez 11amp82424amp82421amp8242amp8242terphenyl2amp82425amp8242dicarboxylicaciddimethylsulfoxided6disolvate
_version_ 1725979520570228736

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