Passion fruit seed oil: extraction and subsequent transesterification reaction

This work aims to remove the oil from passion fruit seeds using ethanol as solvent and then to carry out the transesterification of the product from the extraction step (oil + ethanol). The effects of operational variables in the ultrasound-assisted extraction (UAE) were evaluated and traditional e...

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Main Authors: T.B. Massa, I.J. Iwassa, N. Stevanato, V.A.S. Garcia, C. Silva
Format: Article
Language:English
Published: Consejo Superior de Investigaciones Científicas 2021-06-01
Series:Grasas y Aceites
Subjects:
Online Access:https://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/1876
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spelling doaj-358126c6099845ca8ef9b93bc0e1250e2021-06-28T11:35:53ZengConsejo Superior de Investigaciones CientíficasGrasas y Aceites0017-34951988-42142021-06-0172210.3989/gya.0442201Passion fruit seed oil: extraction and subsequent transesterification reactionT.B. Massa0I.J. Iwassa1N. Stevanato2V.A.S. Garcia3C. Silva4Programa de Pós-graduação em Engenharia Química, Universidade Estadual de Maringá (UEM)Programa de Pós-graduação em Engenharia Química, Universidade Estadual de Maringá (UEM)Programa de Pós-graduação em Engenharia Química, Universidade Estadual de Maringá (UEM)Departamento de Engenharia (FAEN), Engenharia de Alimentos, Universidade Federal da Grande Dourados (UFGD)Programa de Pós-graduação em Engenharia Química, Universidade Estadual de Maringá (UEM) - Departamento de Tecnologia, Universidade Estadual de Maringá (UEM) This work aims to remove the oil from passion fruit seeds using ethanol as solvent and then to carry out the transesterification of the product from the extraction step (oil + ethanol). The effects of operational variables in the ultrasound-assisted extraction (UAE) were evaluated and traditional extraction was performed for comparison. The extraction product was directed to the reaction step using an enzymatic catalyst. UAE provided oil yield from 12.32 to 21.76%, and the maximum value (73.7% of the traditional extraction yield) was obtained at 60 °C and 50 min using a solvent-to-seed ratio of 4. Oil removal was favored by increases in the investigated variables. g-tocopherol, δ-tocopherol and a high concentration of polyunsaturated fatty acids were identified in the oils. The oil obtained by UAE presented higher phytosterol contents. From the reaction step, samples were obtained with higher concentrations of ethyl esters, in addition to emulsifiers (diglycerides and monoglycerides). https://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/1876EmulsifiersEthanolEthyl estersOil yieldUltrasound
collection DOAJ
language English
format Article
sources DOAJ
author T.B. Massa
I.J. Iwassa
N. Stevanato
V.A.S. Garcia
C. Silva
spellingShingle T.B. Massa
I.J. Iwassa
N. Stevanato
V.A.S. Garcia
C. Silva
Passion fruit seed oil: extraction and subsequent transesterification reaction
Grasas y Aceites
Emulsifiers
Ethanol
Ethyl esters
Oil yield
Ultrasound
author_facet T.B. Massa
I.J. Iwassa
N. Stevanato
V.A.S. Garcia
C. Silva
author_sort T.B. Massa
title Passion fruit seed oil: extraction and subsequent transesterification reaction
title_short Passion fruit seed oil: extraction and subsequent transesterification reaction
title_full Passion fruit seed oil: extraction and subsequent transesterification reaction
title_fullStr Passion fruit seed oil: extraction and subsequent transesterification reaction
title_full_unstemmed Passion fruit seed oil: extraction and subsequent transesterification reaction
title_sort passion fruit seed oil: extraction and subsequent transesterification reaction
publisher Consejo Superior de Investigaciones Científicas
series Grasas y Aceites
issn 0017-3495
1988-4214
publishDate 2021-06-01
description This work aims to remove the oil from passion fruit seeds using ethanol as solvent and then to carry out the transesterification of the product from the extraction step (oil + ethanol). The effects of operational variables in the ultrasound-assisted extraction (UAE) were evaluated and traditional extraction was performed for comparison. The extraction product was directed to the reaction step using an enzymatic catalyst. UAE provided oil yield from 12.32 to 21.76%, and the maximum value (73.7% of the traditional extraction yield) was obtained at 60 °C and 50 min using a solvent-to-seed ratio of 4. Oil removal was favored by increases in the investigated variables. g-tocopherol, δ-tocopherol and a high concentration of polyunsaturated fatty acids were identified in the oils. The oil obtained by UAE presented higher phytosterol contents. From the reaction step, samples were obtained with higher concentrations of ethyl esters, in addition to emulsifiers (diglycerides and monoglycerides).
topic Emulsifiers
Ethanol
Ethyl esters
Oil yield
Ultrasound
url https://grasasyaceites.revistas.csic.es/index.php/grasasyaceites/article/view/1876
work_keys_str_mv AT tbmassa passionfruitseedoilextractionandsubsequenttransesterificationreaction
AT ijiwassa passionfruitseedoilextractionandsubsequenttransesterificationreaction
AT nstevanato passionfruitseedoilextractionandsubsequenttransesterificationreaction
AT vasgarcia passionfruitseedoilextractionandsubsequenttransesterificationreaction
AT csilva passionfruitseedoilextractionandsubsequenttransesterificationreaction
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