X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes
The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the s...
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2021-04-01
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| Series: | Data in Brief |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S2352340921002560 |
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doaj-354ce5e1060c499cb01e54a03834bfd52021-04-26T05:56:53ZengElsevierData in Brief2352-34092021-04-0135106972X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routesGaspar Darin0Kengo Imakuma1Rafael Trautwein Santiago2Klebson Lucenildo Da Silva3Luiz Fernardo Cótica4Martin Fabián5Jan Valíček6Horst Hahn7Vladimír Šepelák8Nuclear and Energy Research Institute, IPEN/CNEN-SP, 05508-000 São Paulo, BrazilNuclear and Energy Research Institute, IPEN/CNEN-SP, 05508-000 São Paulo, BrazilPhysics Department, State University of Maringá, 87020-900 Maringá, BrazilPhysics Department, State University of Maringá, 87020-900 Maringá, Brazil; Institute of Geotechnics, Slovak Academy of Sciences, 04001, Košice, Slovakia; Institute of Nanotechnology, Karlsruhe Institute of Technology, 76344, Eggenstein-Leopoldshafen, Germany; Corresponding author at: Physics Department, State University of Maringá, 87020-900 Maringá, Brazil.Physics Department, State University of Maringá, 87020-900 Maringá, BrazilInstitute of Geotechnics, Slovak Academy of Sciences, 04001, Košice, SlovakiaFaculty of Technology, College of Technology and Business in České Budějovice, 37001 České Budějovice, Czech Republic; Faculty of Engineering, Slovak University of Agriculture, 94976 Nitra, SlovakiaInstitute of Nanotechnology, Karlsruhe Institute of Technology, 76344, Eggenstein-Leopoldshafen, GermanyInstitute of Geotechnics, Slovak Academy of Sciences, 04001, Košice, Slovakia; Institute of Nanotechnology, Karlsruhe Institute of Technology, 76344, Eggenstein-Leopoldshafen, Germany; Faculty of Technology, College of Technology and Business in České Budějovice, 37001 České Budějovice, Czech RepublicThe datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid precursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated 3Gd2O3 + UO2 mixture measured in air at a heat rate of 10 K/min.http://www.sciencedirect.com/science/article/pii/S2352340921002560Gd6UO12Rietveld refinementXRDThermal analysisMechanochemistry |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Gaspar Darin Kengo Imakuma Rafael Trautwein Santiago Klebson Lucenildo Da Silva Luiz Fernardo Cótica Martin Fabián Jan Valíček Horst Hahn Vladimír Šepelák |
| spellingShingle |
Gaspar Darin Kengo Imakuma Rafael Trautwein Santiago Klebson Lucenildo Da Silva Luiz Fernardo Cótica Martin Fabián Jan Valíček Horst Hahn Vladimír Šepelák X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes Data in Brief Gd6UO12 Rietveld refinement XRD Thermal analysis Mechanochemistry |
| author_facet |
Gaspar Darin Kengo Imakuma Rafael Trautwein Santiago Klebson Lucenildo Da Silva Luiz Fernardo Cótica Martin Fabián Jan Valíček Horst Hahn Vladimír Šepelák |
| author_sort |
Gaspar Darin |
| title |
X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes |
| title_short |
X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes |
| title_full |
X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes |
| title_fullStr |
X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes |
| title_full_unstemmed |
X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical−thermal routes |
| title_sort |
x-ray diffraction and thermoanalytical datasets of precursors of the gd6uo12-δ phase processed by combined mechanochemical−thermal routes |
| publisher |
Elsevier |
| series |
Data in Brief |
| issn |
2352-3409 |
| publishDate |
2021-04-01 |
| description |
The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid precursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated 3Gd2O3 + UO2 mixture measured in air at a heat rate of 10 K/min. |
| topic |
Gd6UO12 Rietveld refinement XRD Thermal analysis Mechanochemistry |
| url |
http://www.sciencedirect.com/science/article/pii/S2352340921002560 |
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