Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites
Nanoparticles of the TiO2/ZnO composite photocatalysts were prepared via sol-gel process. The crystalline structure, morphology, thermal stability, and pore structure properties of the composite photocatalysts were characterized by XRD, FE-SEM, TG-DTA, and N2 physical adsorption measurements. The ph...
Main Authors: | , , , , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Hindawi Limited
2013-01-01
|
Series: | Journal of Nanomaterials |
Online Access: | http://dx.doi.org/10.1155/2013/321459 |
id |
doaj-3488fde9fe7b4122ba44f44303b46498 |
---|---|
record_format |
Article |
spelling |
doaj-3488fde9fe7b4122ba44f44303b464982020-11-25T00:14:24ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292013-01-01201310.1155/2013/321459321459Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO NanocompositesLiqin Wang0Xiujun Fu1Yang Han2E. Chang3Haitao Wu4Haiying Wang5Kuiying Li6Xiaowen Qi7Hebei Key Laboratory of Applied Chemistry, College of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, ChinaHebei Key Laboratory of Applied Chemistry, College of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, ChinaHebei Key Laboratory of Applied Chemistry, College of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, ChinaHebei Key Laboratory of Applied Chemistry, College of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, ChinaHebei Key Laboratory of Applied Chemistry, College of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, ChinaHebei Key Laboratory of Applied Chemistry, College of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, ChinaState Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao 066004, ChinaCollege of Mechanical Engineering, Yanshan University, Qinhuangdao 066004, ChinaNanoparticles of the TiO2/ZnO composite photocatalysts were prepared via sol-gel process. The crystalline structure, morphology, thermal stability, and pore structure properties of the composite photocatalysts were characterized by XRD, FE-SEM, TG-DTA, and N2 physical adsorption measurements. The photocatalytic activity of the composite catalysts was evaluated by photocatalytic degradation reaction of methyl orange (MO) in aqueous solution. The best preparation parameters for the composite photocatalysts were obtained through systematical experiments. Furthermore, the photocatalytic degradation reaction of aqueous MO solution followed the first-order reaction kinetics; the relative equation can be described as ln(C0/C)=0.5689t, and the calculated correlation constant (R2) is 0.9937 for the calibration curve.http://dx.doi.org/10.1155/2013/321459 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Liqin Wang Xiujun Fu Yang Han E. Chang Haitao Wu Haiying Wang Kuiying Li Xiaowen Qi |
spellingShingle |
Liqin Wang Xiujun Fu Yang Han E. Chang Haitao Wu Haiying Wang Kuiying Li Xiaowen Qi Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites Journal of Nanomaterials |
author_facet |
Liqin Wang Xiujun Fu Yang Han E. Chang Haitao Wu Haiying Wang Kuiying Li Xiaowen Qi |
author_sort |
Liqin Wang |
title |
Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites |
title_short |
Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites |
title_full |
Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites |
title_fullStr |
Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites |
title_full_unstemmed |
Preparation, Characterization, and Photocatalytic Activity of TiO2/ZnO Nanocomposites |
title_sort |
preparation, characterization, and photocatalytic activity of tio2/zno nanocomposites |
publisher |
Hindawi Limited |
series |
Journal of Nanomaterials |
issn |
1687-4110 1687-4129 |
publishDate |
2013-01-01 |
description |
Nanoparticles of the TiO2/ZnO composite photocatalysts were prepared via sol-gel process. The crystalline structure, morphology, thermal stability, and pore structure properties of the composite photocatalysts were characterized by XRD, FE-SEM, TG-DTA, and N2 physical adsorption measurements. The photocatalytic activity of the composite catalysts was evaluated by photocatalytic degradation reaction of methyl orange (MO) in aqueous solution. The best preparation parameters for the composite photocatalysts were obtained through systematical experiments. Furthermore, the photocatalytic degradation reaction of aqueous MO solution followed the first-order reaction kinetics; the relative equation can be described as ln(C0/C)=0.5689t, and the calculated correlation constant (R2) is 0.9937 for the calibration curve. |
url |
http://dx.doi.org/10.1155/2013/321459 |
work_keys_str_mv |
AT liqinwang preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT xiujunfu preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT yanghan preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT echang preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT haitaowu preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT haiyingwang preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT kuiyingli preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites AT xiaowenqi preparationcharacterizationandphotocatalyticactivityoftio2znonanocomposites |
_version_ |
1725390760802516992 |