Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets

Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets

This work presents an electroanalytical method for the determination of moxifloxacin (MOXI) in tablets by its interaction with Cu(II) ion and subsequent electrochemical reduction at hang- ing mercury drop electrode (HMDE). A well-defined reduction peak at -0.21 V vs. Ag/AgCl in Phosphate buffer 0.04...

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Main Authors: Magno Trindade, P. A. C. Cunha, Tatiane Alfonso de Araujo, Glaucia Maria Silva, Valdir S. Ferreira
Format: Article
Language:English
Published: Universidade Estadual Paulista 2018-09-01
Series:Eclética Química
Online Access:https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/405
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spelling doaj-33f26d1f9cb14112a272af7b43cbf0212020-11-24T22:11:28ZengUniversidade Estadual PaulistaEclética Química1678-46182018-09-01311313810.26850/1678-4618eqj.v31.1.2006.p31-38405Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tabletsMagno Trindade0P. A. C. Cunha1Tatiane Alfonso de Araujo2Glaucia Maria Silva3Valdir S. Ferreira4Departamento de Química-CCET, Av Filinto Muller 1555, Caixa Postal 549, CEP 79074-460, Campo Grande, Mato Grosso do Sul, Brasil.Departamento de Química-CCET, Av Filinto Muller 1555, Caixa Postal 549, CEP 79074-460, Campo Grande, Mato Grosso do Sul, Brasil.Departamento de Química, Faculdade de Filosofia, Ciências e Letras de Ribeirão Preto/USP, Av. Bandeirantes, 3900, CEP 14040-901, Ribeirão Preto, São Paulo, Brasil.Departamento de Química, Faculdade de Filosofia, Ciências e Letras de Ribeirão Preto/USP, Av. Bandeirantes, 3900, CEP 14040-901, Ribeirão Preto, São Paulo, Brasil.Departamento de Química-CCET, Av Filinto Muller 1555, Caixa Postal 549, CEP 79074-460, Campo Grande, Mato Grosso do Sul, Brasil.This work presents an electroanalytical method for the determination of moxifloxacin (MOXI) in tablets by its interaction with Cu(II) ion and subsequent electrochemical reduction at hang- ing mercury drop electrode (HMDE). A well-defined reduction peak at -0.21 V vs. Ag/AgCl in Phosphate buffer 0.04 mol L -1 pH 8.0 was observed for the complex reduction MOXI-Cu(II), using square-wave voltammetry (SWV). Using a 10 s of accumulation time at -0.40 V was found a limit detection of 3.60x10 -8 mol l -1 . The obtained results have shown good agreement with those obtained by spectrophotometric method.https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/405
collection DOAJ
language English
format Article
sources DOAJ
author Magno Trindade
P. A. C. Cunha
Tatiane Alfonso de Araujo
Glaucia Maria Silva
Valdir S. Ferreira
spellingShingle Magno Trindade
P. A. C. Cunha
Tatiane Alfonso de Araujo
Glaucia Maria Silva
Valdir S. Ferreira
Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets
Eclética Química
author_facet Magno Trindade
P. A. C. Cunha
Tatiane Alfonso de Araujo
Glaucia Maria Silva
Valdir S. Ferreira
author_sort Magno Trindade
title Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets
title_short Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets
title_full Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets
title_fullStr Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets
title_full_unstemmed Interaction study of moxifloxacin with Cu(II) ion using square-wave voltammetry and its application in the determination in tablets
title_sort interaction study of moxifloxacin with cu(ii) ion using square-wave voltammetry and its application in the determination in tablets
publisher Universidade Estadual Paulista
series Eclética Química
issn 1678-4618
publishDate 2018-09-01
description This work presents an electroanalytical method for the determination of moxifloxacin (MOXI) in tablets by its interaction with Cu(II) ion and subsequent electrochemical reduction at hang- ing mercury drop electrode (HMDE). A well-defined reduction peak at -0.21 V vs. Ag/AgCl in Phosphate buffer 0.04 mol L -1 pH 8.0 was observed for the complex reduction MOXI-Cu(II), using square-wave voltammetry (SWV). Using a 10 s of accumulation time at -0.40 V was found a limit detection of 3.60x10 -8 mol l -1 . The obtained results have shown good agreement with those obtained by spectrophotometric method.
url https://revista.iq.unesp.br/ojs/index.php/ecletica/article/view/405
work_keys_str_mv AT magnotrindade interactionstudyofmoxifloxacinwithcuiiionusingsquarewavevoltammetryanditsapplicationinthedeterminationintablets
AT paccunha interactionstudyofmoxifloxacinwithcuiiionusingsquarewavevoltammetryanditsapplicationinthedeterminationintablets
AT tatianealfonsodearaujo interactionstudyofmoxifloxacinwithcuiiionusingsquarewavevoltammetryanditsapplicationinthedeterminationintablets
AT glauciamariasilva interactionstudyofmoxifloxacinwithcuiiionusingsquarewavevoltammetryanditsapplicationinthedeterminationintablets
AT valdirsferreira interactionstudyofmoxifloxacinwithcuiiionusingsquarewavevoltammetryanditsapplicationinthedeterminationintablets
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