2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol

2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol

The reaction of 2-aminoethanol and iodopentafluorobenzene in the presence of K2CO3 gave the title compound, C8H6F4INO, in high yield. The structure is characterized by double layers of molecules linked by O—H...O and N—H...O hydrogen bonds, and linear C—I...F [I...F = 3...

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Main Authors: Pierangelo Metrangolo, Franck Meyer, Tullio Pilati, Giuseppe Resnati
Format: Article
Language:English
Published: International Union of Crystallography 2008-01-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536807064197
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spelling doaj-312cdd3e3b7e43c7a184d0ea214ba8182020-11-25T00:31:14ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-01-01641o211o21110.1107/S16005368070641972-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanolPierangelo MetrangoloFranck MeyerTullio PilatiGiuseppe ResnatiThe reaction of 2-aminoethanol and iodopentafluorobenzene in the presence of K2CO3 gave the title compound, C8H6F4INO, in high yield. The structure is characterized by double layers of molecules linked by O—H...O and N—H...O hydrogen bonds, and linear C—I...F [I...F = 3.049 (2) Å] and bent C—I...I [I...I = 3.9388 (7) Å] interactions between pairs of nearly parallel iodotetrafluorophenyl groups. No O...I or N...I halogen bonding is found.http://scripts.iucr.org/cgi-bin/paper?S1600536807064197
collection DOAJ
language English
format Article
sources DOAJ
author Pierangelo Metrangolo
Franck Meyer
Tullio Pilati
Giuseppe Resnati
spellingShingle Pierangelo Metrangolo
Franck Meyer
Tullio Pilati
Giuseppe Resnati
2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol
Acta Crystallographica Section E
author_facet Pierangelo Metrangolo
Franck Meyer
Tullio Pilati
Giuseppe Resnati
author_sort Pierangelo Metrangolo
title 2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol
title_short 2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol
title_full 2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol
title_fullStr 2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol
title_full_unstemmed 2-(2,3,5,6-Tetrafluoro-4-iodoanilino)ethanol
title_sort 2-(2,3,5,6-tetrafluoro-4-iodoanilino)ethanol
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2008-01-01
description The reaction of 2-aminoethanol and iodopentafluorobenzene in the presence of K2CO3 gave the title compound, C8H6F4INO, in high yield. The structure is characterized by double layers of molecules linked by O—H...O and N—H...O hydrogen bonds, and linear C—I...F [I...F = 3.049 (2) Å] and bent C—I...I [I...I = 3.9388 (7) Å] interactions between pairs of nearly parallel iodotetrafluorophenyl groups. No O...I or N...I halogen bonding is found.
url http://scripts.iucr.org/cgi-bin/paper?S1600536807064197
work_keys_str_mv AT pierangelometrangolo 22356tetrafluoro4iodoanilinoethanol
AT franckmeyer 22356tetrafluoro4iodoanilinoethanol
AT tulliopilati 22356tetrafluoro4iodoanilinoethanol
AT giusepperesnati 22356tetrafluoro4iodoanilinoethanol
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