Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract

Abstract A simple, inexpensive, and rapid method for simultaneous determination of trigonelline, caffeine, and chlorogenic acid from green coffee bean extract was proposed based on salting‐out assisted liquid–liquid extraction, using QuEChERS salt and acetonitrile followed by UV‐Vis analysis. The pr...

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Main Authors:	Minaleshewa Atlabachew, Atakilt Abebe, Tessera Alemneh Wubieneh, Yilak Tefera Habtemariam
Format:	Article
Language:	English
Published:	Wiley 2021-09-01
Series:	Food Science & Nutrition
Subjects:	caffeine chlorogenic acid green coffee QuEChERS salt salting‐out assisted liquid–liquid extraction trigonelline
Online Access:	https://doi.org/10.1002/fsn3.2456

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spelling	doaj-2de30740d1584535ad6f7585ee92efff2021-09-15T07:28:34ZengWileyFood Science & Nutrition2048-71772021-09-01995028503510.1002/fsn3.2456Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extractMinaleshewa Atlabachew0Atakilt Abebe1Tessera Alemneh Wubieneh2Yilak Tefera Habtemariam3Chemistry Department Science College Bahir Dar University Bahir Dar EthiopiaChemistry Department Science College Bahir Dar University Bahir Dar EthiopiaMaterial Science and Engineering Department Science College Bahir Dar University Bahir Dar EthiopiaChemistry Department Science College Bahir Dar University Bahir Dar EthiopiaAbstract A simple, inexpensive, and rapid method for simultaneous determination of trigonelline, caffeine, and chlorogenic acid from green coffee bean extract was proposed based on salting‐out assisted liquid–liquid extraction, using QuEChERS salt and acetonitrile followed by UV‐Vis analysis. The proposed method represents acceptable linearity for trigonelline (0.9978), caffeine (0.9995), and chlorogenic acid (0.9996) with excellent correlation (0.93 and 0.83) for trigonelline and caffeine, respectively, when compared to RP‐HPLC‐DAD. The proposed method could be used in coffee industries for quality control and geographical origin traceability studies of green coffee samples.https://doi.org/10.1002/fsn3.2456caffeinechlorogenic acidgreen coffeeQuEChERS saltsalting‐out assisted liquid–liquid extractiontrigonelline
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Minaleshewa Atlabachew Atakilt Abebe Tessera Alemneh Wubieneh Yilak Tefera Habtemariam
spellingShingle	Minaleshewa Atlabachew Atakilt Abebe Tessera Alemneh Wubieneh Yilak Tefera Habtemariam Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract Food Science & Nutrition caffeine chlorogenic acid green coffee QuEChERS salt salting‐out assisted liquid–liquid extraction trigonelline
author_facet	Minaleshewa Atlabachew Atakilt Abebe Tessera Alemneh Wubieneh Yilak Tefera Habtemariam
author_sort	Minaleshewa Atlabachew
title	Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract
title_short	Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract
title_full	Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract
title_fullStr	Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract
title_full_unstemmed	Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract
title_sort	rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract
publisher	Wiley
series	Food Science & Nutrition
issn	2048-7177
publishDate	2021-09-01
description	Abstract A simple, inexpensive, and rapid method for simultaneous determination of trigonelline, caffeine, and chlorogenic acid from green coffee bean extract was proposed based on salting‐out assisted liquid–liquid extraction, using QuEChERS salt and acetonitrile followed by UV‐Vis analysis. The proposed method represents acceptable linearity for trigonelline (0.9978), caffeine (0.9995), and chlorogenic acid (0.9996) with excellent correlation (0.93 and 0.83) for trigonelline and caffeine, respectively, when compared to RP‐HPLC‐DAD. The proposed method could be used in coffee industries for quality control and geographical origin traceability studies of green coffee samples.
topic	caffeine chlorogenic acid green coffee QuEChERS salt salting‐out assisted liquid–liquid extraction trigonelline
url	https://doi.org/10.1002/fsn3.2456
work_keys_str_mv	AT minaleshewaatlabachew rapidandsimultaneousdeterminationoftrigonellinecaffeineandchlorogenicacidingreencoffeebeanextract AT atakiltabebe rapidandsimultaneousdeterminationoftrigonellinecaffeineandchlorogenicacidingreencoffeebeanextract AT tesseraalemnehwubieneh rapidandsimultaneousdeterminationoftrigonellinecaffeineandchlorogenicacidingreencoffeebeanextract AT yilakteferahabtemariam rapidandsimultaneousdeterminationoftrigonellinecaffeineandchlorogenicacidingreencoffeebeanextract
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Rapid and simultaneous determination of trigonelline, caffeine, and chlorogenic acid in green coffee bean extract

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