Bis(N-methyl-N-phenylcarbamoyl)disulfane

Bis(N-methyl-N-phenylcarbamoyl)disulfane

The title compound, C16H16N2O2S2, has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of interest to our research program over 30 years ago. We now confirm the proposed molecular structure in whi...

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Bibliographic Details
Main Authors: George Barany, Maren Pink, Alayne L. Schroll
Format: Article
Language:English
Published: International Union of Crystallography 2012-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812016030
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spelling doaj-2d658688662d4df7a7e3c679bbeb3e932020-11-24T22:08:23ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-05-01685o1550o155010.1107/S1600536812016030Bis(N-methyl-N-phenylcarbamoyl)disulfaneGeorge BaranyMaren PinkAlayne L. SchrollThe title compound, C16H16N2O2S2, has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of interest to our research program over 30 years ago. We now confirm the proposed molecular structure in which the molecule exhibits a twofold axis of symmetry through the mid-point of the S—S bond and the two planes defined by the (carbamoyl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].http://scripts.iucr.org/cgi-bin/paper?S1600536812016030
collection DOAJ
language English
format Article
sources DOAJ
author George Barany
Maren Pink
Alayne L. Schroll
spellingShingle George Barany
Maren Pink
Alayne L. Schroll
Bis(N-methyl-N-phenylcarbamoyl)disulfane
Acta Crystallographica Section E
author_facet George Barany
Maren Pink
Alayne L. Schroll
author_sort George Barany
title Bis(N-methyl-N-phenylcarbamoyl)disulfane
title_short Bis(N-methyl-N-phenylcarbamoyl)disulfane
title_full Bis(N-methyl-N-phenylcarbamoyl)disulfane
title_fullStr Bis(N-methyl-N-phenylcarbamoyl)disulfane
title_full_unstemmed Bis(N-methyl-N-phenylcarbamoyl)disulfane
title_sort bis(n-methyl-n-phenylcarbamoyl)disulfane
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-05-01
description The title compound, C16H16N2O2S2, has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of interest to our research program over 30 years ago. We now confirm the proposed molecular structure in which the molecule exhibits a twofold axis of symmetry through the mid-point of the S—S bond and the two planes defined by the (carbamoyl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].
url http://scripts.iucr.org/cgi-bin/paper?S1600536812016030
work_keys_str_mv AT georgebarany bisnmethylnphenylcarbamoyldisulfane
AT marenpink bisnmethylnphenylcarbamoyldisulfane
AT alaynelschroll bisnmethylnphenylcarbamoyldisulfane
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