Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel

The kinetics of ferritic transformation and the corresponding microstructural evolution in 0.17C-3.1Mn-1.6Al-0.04Nb-0.22Mo-0.22Si medium-Mn steel during isothermal annealing was investigated in dilatometric studies. The material was subjected to thermal and thermo-mechanical treatments aimed at obta...

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Main Authors: Adam Skowronek, Mateusz Morawiec, Aleksandra Kozłowska, Wojciech Pakieła
Format: Article
Language:English
Published: MDPI AG 2020-12-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/13/24/5817
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spelling doaj-2d60735b31a54ebc93e666b54709fbfe2020-12-21T00:01:24ZengMDPI AGMaterials1996-19442020-12-01135817581710.3390/ma13245817Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al SteelAdam Skowronek0Mateusz Morawiec1Aleksandra Kozłowska2Wojciech Pakieła3Department of Engineering Materials and Biomaterials, Silesian University of Technology, 18a Konarskiego Street, 44-100 Gliwice, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, 18a Konarskiego Street, 44-100 Gliwice, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, 18a Konarskiego Street, 44-100 Gliwice, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, 18a Konarskiego Street, 44-100 Gliwice, PolandThe kinetics of ferritic transformation and the corresponding microstructural evolution in 0.17C-3.1Mn-1.6Al-0.04Nb-0.22Mo-0.22Si medium-Mn steel during isothermal annealing was investigated in dilatometric studies. The material was subjected to thermal and thermo-mechanical treatments aimed at obtaining, by the austenite → ferrite transformation, a sufficient fraction of ferrite to stabilize the retained austenite by C and eventual Mn partitioning. The samples were isothermally held for 5 h in a temperature range from 600 to 750 °C to simulate simplified temperature conditions of an industrial coiling process following hot rolling. Some of the samples were plastically deformed at a temperature of 900 °C before isothermal holding in order to study the effect of hot deformation on the kinetics of phase transformations. After the dilatometric investigations the material was subjected to light and scanning electron microscopy to reveal relationships between the holding temperature, deformation and microstructure evolution. Hardness tests were performed to assess the mechanical behavior. A significant effect of manganese in slowing down diffusional transformations during the cooling of steel was found. The influence of austenite deformation on the kinetics of austenite to ferrite transformation was noted. The plastically deformed samples showed an accelerated start of ferritic transformation and the extension of its range. During dilatometric tests, low-range dynamic ferritic transformation was recorded, which was also confirmed by the microscopic tests.https://www.mdpi.com/1996-1944/13/24/5817medium-Mn steelcoiling simulationdilatometryretained austeniteinter-critical holding
collection DOAJ
language English
format Article
sources DOAJ
author Adam Skowronek
Mateusz Morawiec
Aleksandra Kozłowska
Wojciech Pakieła
spellingShingle Adam Skowronek
Mateusz Morawiec
Aleksandra Kozłowska
Wojciech Pakieła
Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel
Materials
medium-Mn steel
coiling simulation
dilatometry
retained austenite
inter-critical holding
author_facet Adam Skowronek
Mateusz Morawiec
Aleksandra Kozłowska
Wojciech Pakieła
author_sort Adam Skowronek
title Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel
title_short Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel
title_full Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel
title_fullStr Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel
title_full_unstemmed Effect of Hot Deformation on Phase Transformation Kinetics in Isothermally Annealed 3Mn-1.6Al Steel
title_sort effect of hot deformation on phase transformation kinetics in isothermally annealed 3mn-1.6al steel
publisher MDPI AG
series Materials
issn 1996-1944
publishDate 2020-12-01
description The kinetics of ferritic transformation and the corresponding microstructural evolution in 0.17C-3.1Mn-1.6Al-0.04Nb-0.22Mo-0.22Si medium-Mn steel during isothermal annealing was investigated in dilatometric studies. The material was subjected to thermal and thermo-mechanical treatments aimed at obtaining, by the austenite → ferrite transformation, a sufficient fraction of ferrite to stabilize the retained austenite by C and eventual Mn partitioning. The samples were isothermally held for 5 h in a temperature range from 600 to 750 °C to simulate simplified temperature conditions of an industrial coiling process following hot rolling. Some of the samples were plastically deformed at a temperature of 900 °C before isothermal holding in order to study the effect of hot deformation on the kinetics of phase transformations. After the dilatometric investigations the material was subjected to light and scanning electron microscopy to reveal relationships between the holding temperature, deformation and microstructure evolution. Hardness tests were performed to assess the mechanical behavior. A significant effect of manganese in slowing down diffusional transformations during the cooling of steel was found. The influence of austenite deformation on the kinetics of austenite to ferrite transformation was noted. The plastically deformed samples showed an accelerated start of ferritic transformation and the extension of its range. During dilatometric tests, low-range dynamic ferritic transformation was recorded, which was also confirmed by the microscopic tests.
topic medium-Mn steel
coiling simulation
dilatometry
retained austenite
inter-critical holding
url https://www.mdpi.com/1996-1944/13/24/5817
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