Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source

A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO4) nanocrystals with decavanadate (K6V10O28·9H2O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a r...

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Main Authors:	Quanguo Li, Wenli Zuo, Feng Li
Format:	Article
Language:	English
Published:	Hindawi Limited 2013-01-01
Series:	The Scientific World Journal
Online Access:	http://dx.doi.org/10.1155/2013/127816

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spelling	doaj-2ce02a04053d4c2b8e2378f80bf20eed2020-11-24T21:32:21ZengHindawi LimitedThe Scientific World Journal1537-744X2013-01-01201310.1155/2013/127816127816Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium SourceQuanguo Li0Wenli Zuo1Feng Li2College of Chemistry, Key Lab of Environment Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemistry, Key Lab of Environment Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan 411105, ChinaCollege of Chemistry, Key Lab of Environment Friendly Chemistry and Application in Ministry of Education, Xiangtan University, Xiangtan 411105, ChinaA new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO4) nanocrystals with decavanadate (K6V10O28·9H2O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems play important roles in determining the morphologies and growth process of the SmVO4 products. The products have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), photoluminescence spectra (PL), and UV-Vis spectroscopy.http://dx.doi.org/10.1155/2013/127816
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Quanguo Li Wenli Zuo Feng Li
spellingShingle	Quanguo Li Wenli Zuo Feng Li Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source The Scientific World Journal
author_facet	Quanguo Li Wenli Zuo Feng Li
author_sort	Quanguo Li
title	Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_short	Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_full	Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_fullStr	Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_full_unstemmed	Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source
title_sort	chelating ligand-mediated hydrothermal synthesis of samarium orthovanadate with decavanadate as vanadium source
publisher	Hindawi Limited
series	The Scientific World Journal
issn	1537-744X
publishDate	2013-01-01
description	A new ethylenediaminetetraacetic acid- (EDTA-) mediated hydrothermal route to prepare chrysanthemum-shaped samarium orthovanadate (SmVO4) nanocrystals with decavanadate (K6V10O28·9H2O) as vanadium source has been developed. The present hydrothermal approach is simple and reproducible and employs a relatively mild reaction temperature. The EDTA, pH value, and temperature of the reaction systems play important roles in determining the morphologies and growth process of the SmVO4 products. The products have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), photoluminescence spectra (PL), and UV-Vis spectroscopy.
url	http://dx.doi.org/10.1155/2013/127816
work_keys_str_mv	AT quanguoli chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource AT wenlizuo chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource AT fengli chelatingligandmediatedhydrothermalsynthesisofsamariumorthovanadatewithdecavanadateasvanadiumsource
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Chelating Ligand-Mediated Hydrothermal Synthesis of Samarium Orthovanadate with Decavanadate as Vanadium Source

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