5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione

5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione

In the title molecule, C23H25FN4O7, the dihedral angle between the indole skeleton (r.m.s. deviation = 0.022 Å) and the triazole moiety is 74.67 (7)°. The molecules pack in a three-dimensional network in the crystal, being linked by C—H...O and N—H...O hydrogen bonds.

Bibliographic Details
Main Authors: Fatima-Zahrae Qachchachi, Joel T. Mague, Youssef Kandri Rodi, Amal Haoudi, El Mestafa El Hadrami, El Mokhtar Essassi
Format: Article
Language:English
Published: International Union of Crystallography 2017-05-01
Series:IUCrData
Subjects:
crystal structure
triazole
isatin
hydrogen bond
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2414314617007398
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record_format Article
spelling doaj-283f16056d774f2fa5a7ffc8102250092020-11-25T00:14:07ZengInternational Union of CrystallographyIUCrData2414-31462017-05-0125x17073910.1107/S2414314617007398hb41455-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dioneFatima-Zahrae Qachchachi0Joel T. Mague1Youssef Kandri Rodi2Amal Haoudi3El Mestafa El Hadrami4El Mokhtar Essassi5Laboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoDepartment of Chemistry, Tulane University, New Orleans, LA 70118, USALaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Appliquée, Université Sidi Mohamed Ben Abdallah, Faculté des Sciences et Techniques, Route d'Imouzzer, BP 2202, Fez, MoroccoLaboratoire de Chimie Organique Hétérocyclique URAC 21, Pôle de Compétence Pharmacochimie, Av. Ibn Battouta, BP 1014, Faculté des Sciences, Université Mohammed V, Rabat, MoroccoIn the title molecule, C23H25FN4O7, the dihedral angle between the indole skeleton (r.m.s. deviation = 0.022 Å) and the triazole moiety is 74.67 (7)°. The molecules pack in a three-dimensional network in the crystal, being linked by C—H...O and N—H...O hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S2414314617007398crystal structuretriazoleisatinhydrogen bond
collection DOAJ
language English
format Article
sources DOAJ
author Fatima-Zahrae Qachchachi
Joel T. Mague
Youssef Kandri Rodi
Amal Haoudi
El Mestafa El Hadrami
El Mokhtar Essassi
spellingShingle Fatima-Zahrae Qachchachi
Joel T. Mague
Youssef Kandri Rodi
Amal Haoudi
El Mestafa El Hadrami
El Mokhtar Essassi
5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
IUCrData
crystal structure
triazole
isatin
hydrogen bond
author_facet Fatima-Zahrae Qachchachi
Joel T. Mague
Youssef Kandri Rodi
Amal Haoudi
El Mestafa El Hadrami
El Mokhtar Essassi
author_sort Fatima-Zahrae Qachchachi
title 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
title_short 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
title_full 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
title_fullStr 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
title_full_unstemmed 5-Fluoro-1-[(1-{[(1S,2R,6R,8S,9R)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1H-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1H-indole-2,3-dione
title_sort 5-fluoro-1-[(1-{[(1s,2r,6r,8s,9r)-4,4,11,11-tetramethyl-3,5,7,10,12-pentaoxatricyclo[7.3.0.02,6]dodecan-8-yl]methyl}-1h-1,2,3-triazol-4-yl)methyl]-2,3-dihydro-1h-indole-2,3-dione
publisher International Union of Crystallography
series IUCrData
issn 2414-3146
publishDate 2017-05-01
description In the title molecule, C23H25FN4O7, the dihedral angle between the indole skeleton (r.m.s. deviation = 0.022 Å) and the triazole moiety is 74.67 (7)°. The molecules pack in a three-dimensional network in the crystal, being linked by C—H...O and N—H...O hydrogen bonds.
topic crystal structure
triazole
isatin
hydrogen bond
url http://scripts.iucr.org/cgi-bin/paper?S2414314617007398
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AT joeltmague 5fluoro111s2r6r8s9r441111tetramethyl3571012pentaoxatricyclo730026dodecan8ylmethyl1h123triazol4ylmethyl23dihydro1hindole23dione
AT youssefkandrirodi 5fluoro111s2r6r8s9r441111tetramethyl3571012pentaoxatricyclo730026dodecan8ylmethyl1h123triazol4ylmethyl23dihydro1hindole23dione
AT amalhaoudi 5fluoro111s2r6r8s9r441111tetramethyl3571012pentaoxatricyclo730026dodecan8ylmethyl1h123triazol4ylmethyl23dihydro1hindole23dione
AT elmestafaelhadrami 5fluoro111s2r6r8s9r441111tetramethyl3571012pentaoxatricyclo730026dodecan8ylmethyl1h123triazol4ylmethyl23dihydro1hindole23dione
AT elmokhtaressassi 5fluoro111s2r6r8s9r441111tetramethyl3571012pentaoxatricyclo730026dodecan8ylmethyl1h123triazol4ylmethyl23dihydro1hindole23dione
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