3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione

3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione

The title compound, C13H10N4O2S, was prepared through a cyclization reaction of 1,10-phenanthroline-5,6-dione and thiourea. The dihedral angle between the pyridine rings is 8.22 (2)°. In the crystal, molecules are connected by N—H...O, O—H...N,...

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Main Authors: Hua Wang, Peng Mei, Wen-Yi Chu, Zhi-Zhong Sun, Yan-Jun Hou
Format: Article
Language:English
Published: International Union of Crystallography 2012-01-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811053967
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spelling doaj-275c1c2dc3974f64b033342c9fed868d2020-11-25T02:40:40ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-01-01681o208o20810.1107/S16005368110539673a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thioneHua WangPeng MeiWen-Yi ChuZhi-Zhong SunYan-Jun HouThe title compound, C13H10N4O2S, was prepared through a cyclization reaction of 1,10-phenanthroline-5,6-dione and thiourea. The dihedral angle between the pyridine rings is 8.22 (2)°. In the crystal, molecules are connected by N—H...O, O—H...N, N—H...S and O—H...S hydrogen bonds, forming a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S1600536811053967
collection DOAJ
language English
format Article
sources DOAJ
author Hua Wang
Peng Mei
Wen-Yi Chu
Zhi-Zhong Sun
Yan-Jun Hou
spellingShingle Hua Wang
Peng Mei
Wen-Yi Chu
Zhi-Zhong Sun
Yan-Jun Hou
3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione
Acta Crystallographica Section E
author_facet Hua Wang
Peng Mei
Wen-Yi Chu
Zhi-Zhong Sun
Yan-Jun Hou
author_sort Hua Wang
title 3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione
title_short 3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione
title_full 3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione
title_fullStr 3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione
title_full_unstemmed 3a,11b-Dihydroxy-3a,11b-dihydro-1H-imidazo[4,5-f][1,10]phenanthroline-2(3H)-thione
title_sort 3a,11b-dihydroxy-3a,11b-dihydro-1h-imidazo[4,5-f][1,10]phenanthroline-2(3h)-thione
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-01-01
description The title compound, C13H10N4O2S, was prepared through a cyclization reaction of 1,10-phenanthroline-5,6-dione and thiourea. The dihedral angle between the pyridine rings is 8.22 (2)°. In the crystal, molecules are connected by N—H...O, O—H...N, N—H...S and O—H...S hydrogen bonds, forming a three-dimensional network.
url http://scripts.iucr.org/cgi-bin/paper?S1600536811053967
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AT pengmei 3a11bdihydroxy3a11bdihydro1himidazo45f110phenanthroline23hthione
AT wenyichu 3a11bdihydroxy3a11bdihydro1himidazo45f110phenanthroline23hthione
AT zhizhongsun 3a11bdihydroxy3a11bdihydro1himidazo45f110phenanthroline23hthione
AT yanjunhou 3a11bdihydroxy3a11bdihydro1himidazo45f110phenanthroline23hthione
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