11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate

11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate

In the title compound, C22H24N2O2·H2O, the co-crystallized water molecule interacts with the N and O atoms of the molecule through Ow—H...N, Ow—H...O(methyl) and N—H...Ow hydrogen-bonding interactions. These hydrogen bonds, along with the interm...

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Main Authors: Olatomide A. Fadare, Adebomi A. Ikotun, Pius O. Adelani, Craig A. Obafemi
Format: Article
Language:English
Published: International Union of Crystallography 2012-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812016194
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spelling doaj-266a4e50df1c4338a078ac92a28662052020-11-24T20:56:09ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-05-01685o1508o150910.1107/S160053681201619411-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrateOlatomide A. FadareAdebomi A. IkotunPius O. AdelaniCraig A. ObafemiIn the title compound, C22H24N2O2·H2O, the co-crystallized water molecule interacts with the N and O atoms of the molecule through Ow—H...N, Ow—H...O(methyl) and N—H...Ow hydrogen-bonding interactions. These hydrogen bonds, along with the intermolecular N—H...O=C hydrogen-bonding interactions, connect the molecules into a three-dimensional network. The dihedral angle between the two aromatic rings is 65.46 (10)°.http://scripts.iucr.org/cgi-bin/paper?S1600536812016194
collection DOAJ
language English
format Article
sources DOAJ
author Olatomide A. Fadare
Adebomi A. Ikotun
Pius O. Adelani
Craig A. Obafemi
spellingShingle Olatomide A. Fadare
Adebomi A. Ikotun
Pius O. Adelani
Craig A. Obafemi
11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
Acta Crystallographica Section E
author_facet Olatomide A. Fadare
Adebomi A. Ikotun
Pius O. Adelani
Craig A. Obafemi
author_sort Olatomide A. Fadare
title 11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_short 11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_full 11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_fullStr 11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_full_unstemmed 11-(4-Methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_sort 11-(4-methoxyphenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1h-dibenzo[b,e][1,4]diazepin-1-one monohydrate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-05-01
description In the title compound, C22H24N2O2·H2O, the co-crystallized water molecule interacts with the N and O atoms of the molecule through Ow—H...N, Ow—H...O(methyl) and N—H...Ow hydrogen-bonding interactions. These hydrogen bonds, along with the intermolecular N—H...O=C hydrogen-bonding interactions, connect the molecules into a three-dimensional network. The dihedral angle between the two aromatic rings is 65.46 (10)°.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812016194
work_keys_str_mv AT olatomideafadare 114methoxyphenyl33dimethyl23451011hexahydro1hdibenzobe14diazepin1onemonohydrate
AT adebomiaikotun 114methoxyphenyl33dimethyl23451011hexahydro1hdibenzobe14diazepin1onemonohydrate
AT piusoadelani 114methoxyphenyl33dimethyl23451011hexahydro1hdibenzobe14diazepin1onemonohydrate
AT craigaobafemi 114methoxyphenyl33dimethyl23451011hexahydro1hdibenzobe14diazepin1onemonohydrate
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