The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
Deformation of an as-rolled rare earth Mg-2Y-0.6Nd-0.6Zr alloy, at different temperatures, was carried out along the BC (90° anticlockwise rotation of the samples after each ECAP pass) route by equal channel angular pressing (ECAP). The effects of the deformation temperature and the predefo...
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doaj-25378884e573446c820279cb08bb3e2b2020-11-24T21:31:45ZengMDPI AGMaterials1996-19442019-05-01129155410.3390/ma12091554ma12091554The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium AlloyYun Tan0Wei Li1Weiwei Hu2Xiaofang Shi3Liang Tian4College of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaCollege of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaCollege of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaCollege of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaGuizhou Province Technology Innovation Service Center, Guiyang 550004, ChinaDeformation of an as-rolled rare earth Mg-2Y-0.6Nd-0.6Zr alloy, at different temperatures, was carried out along the BC (90° anticlockwise rotation of the samples after each ECAP pass) route by equal channel angular pressing (ECAP). The effects of the deformation temperature and the predeformation on the microstructure of the magnesium alloy were determined by the microstructure examination. The slip systems and texture change of the Mg-2Y-0.6Nd-0.6Zr alloy were investigated by X-ray diffraction (XRD) and electron backscattered diffraction (EBSD), after equal channel angular deformation. The results showed that after seven passes of rolling, the grain size in the Mg-2Y-0.6Nd-0.6Zr alloy was refined to approximately 22 µm and the slip occurred mainly by a cylindrical slip and a pyramidal slip. After one pass of ECAP at 340 °C, the internal average grain size was significantly reduced to 11 µm, the cylindrical diffraction intensity clearly weakened, and the pyramidal diffraction intensity increased. EBSD pole figure analysis revealed that the base texture of the rolled Mg-2Y-0.6Nd-0.6Zr alloy weakened from 24.31 to 11.34 after ECAP. The mechanical properties indicated that the tensile strength and elongation of the rolled Mg-2Y-0.6Nd-0.6Zr alloy reached maximum values, when the deformation temperature was 340 °C.https://www.mdpi.com/1996-1944/12/9/1554Mg-2Y-0.6Nd-0.6Zr alloyequal channel angular pressingpredeformationdeformation temperature |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Yun Tan Wei Li Weiwei Hu Xiaofang Shi Liang Tian |
spellingShingle |
Yun Tan Wei Li Weiwei Hu Xiaofang Shi Liang Tian The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy Materials Mg-2Y-0.6Nd-0.6Zr alloy equal channel angular pressing predeformation deformation temperature |
author_facet |
Yun Tan Wei Li Weiwei Hu Xiaofang Shi Liang Tian |
author_sort |
Yun Tan |
title |
The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy |
title_short |
The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy |
title_full |
The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy |
title_fullStr |
The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy |
title_full_unstemmed |
The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy |
title_sort |
effect of ecap temperature on the microstructure and properties of a rolled rare earth magnesium alloy |
publisher |
MDPI AG |
series |
Materials |
issn |
1996-1944 |
publishDate |
2019-05-01 |
description |
Deformation of an as-rolled rare earth Mg-2Y-0.6Nd-0.6Zr alloy, at different temperatures, was carried out along the BC (90° anticlockwise rotation of the samples after each ECAP pass) route by equal channel angular pressing (ECAP). The effects of the deformation temperature and the predeformation on the microstructure of the magnesium alloy were determined by the microstructure examination. The slip systems and texture change of the Mg-2Y-0.6Nd-0.6Zr alloy were investigated by X-ray diffraction (XRD) and electron backscattered diffraction (EBSD), after equal channel angular deformation. The results showed that after seven passes of rolling, the grain size in the Mg-2Y-0.6Nd-0.6Zr alloy was refined to approximately 22 µm and the slip occurred mainly by a cylindrical slip and a pyramidal slip. After one pass of ECAP at 340 °C, the internal average grain size was significantly reduced to 11 µm, the cylindrical diffraction intensity clearly weakened, and the pyramidal diffraction intensity increased. EBSD pole figure analysis revealed that the base texture of the rolled Mg-2Y-0.6Nd-0.6Zr alloy weakened from 24.31 to 11.34 after ECAP. The mechanical properties indicated that the tensile strength and elongation of the rolled Mg-2Y-0.6Nd-0.6Zr alloy reached maximum values, when the deformation temperature was 340 °C. |
topic |
Mg-2Y-0.6Nd-0.6Zr alloy equal channel angular pressing predeformation deformation temperature |
url |
https://www.mdpi.com/1996-1944/12/9/1554 |
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