The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy

Deformation of an as-rolled rare earth Mg-2Y-0.6Nd-0.6Zr alloy, at different temperatures, was carried out along the BC (90° anticlockwise rotation of the samples after each ECAP pass) route by equal channel angular pressing (ECAP). The effects of the deformation temperature and the predefo...

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Main Authors: Yun Tan, Wei Li, Weiwei Hu, Xiaofang Shi, Liang Tian
Format: Article
Language:English
Published: MDPI AG 2019-05-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/12/9/1554
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spelling doaj-25378884e573446c820279cb08bb3e2b2020-11-24T21:31:45ZengMDPI AGMaterials1996-19442019-05-01129155410.3390/ma12091554ma12091554The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium AlloyYun Tan0Wei Li1Weiwei Hu2Xiaofang Shi3Liang Tian4College of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaCollege of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaCollege of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaCollege of Material and Metallurgy, Guizhou University, Guiyang 550025, ChinaGuizhou Province Technology Innovation Service Center, Guiyang 550004, ChinaDeformation of an as-rolled rare earth Mg-2Y-0.6Nd-0.6Zr alloy, at different temperatures, was carried out along the BC (90° anticlockwise rotation of the samples after each ECAP pass) route by equal channel angular pressing (ECAP). The effects of the deformation temperature and the predeformation on the microstructure of the magnesium alloy were determined by the microstructure examination. The slip systems and texture change of the Mg-2Y-0.6Nd-0.6Zr alloy were investigated by X-ray diffraction (XRD) and electron backscattered diffraction (EBSD), after equal channel angular deformation. The results showed that after seven passes of rolling, the grain size in the Mg-2Y-0.6Nd-0.6Zr alloy was refined to approximately 22 µm and the slip occurred mainly by a cylindrical slip and a pyramidal slip. After one pass of ECAP at 340 °C, the internal average grain size was significantly reduced to 11 µm, the cylindrical diffraction intensity clearly weakened, and the pyramidal diffraction intensity increased. EBSD pole figure analysis revealed that the base texture of the rolled Mg-2Y-0.6Nd-0.6Zr alloy weakened from 24.31 to 11.34 after ECAP. The mechanical properties indicated that the tensile strength and elongation of the rolled Mg-2Y-0.6Nd-0.6Zr alloy reached maximum values, when the deformation temperature was 340 °C.https://www.mdpi.com/1996-1944/12/9/1554Mg-2Y-0.6Nd-0.6Zr alloyequal channel angular pressingpredeformationdeformation temperature
collection DOAJ
language English
format Article
sources DOAJ
author Yun Tan
Wei Li
Weiwei Hu
Xiaofang Shi
Liang Tian
spellingShingle Yun Tan
Wei Li
Weiwei Hu
Xiaofang Shi
Liang Tian
The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
Materials
Mg-2Y-0.6Nd-0.6Zr alloy
equal channel angular pressing
predeformation
deformation temperature
author_facet Yun Tan
Wei Li
Weiwei Hu
Xiaofang Shi
Liang Tian
author_sort Yun Tan
title The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
title_short The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
title_full The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
title_fullStr The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
title_full_unstemmed The Effect of ECAP Temperature on the Microstructure and Properties of a Rolled Rare Earth Magnesium Alloy
title_sort effect of ecap temperature on the microstructure and properties of a rolled rare earth magnesium alloy
publisher MDPI AG
series Materials
issn 1996-1944
publishDate 2019-05-01
description Deformation of an as-rolled rare earth Mg-2Y-0.6Nd-0.6Zr alloy, at different temperatures, was carried out along the BC (90° anticlockwise rotation of the samples after each ECAP pass) route by equal channel angular pressing (ECAP). The effects of the deformation temperature and the predeformation on the microstructure of the magnesium alloy were determined by the microstructure examination. The slip systems and texture change of the Mg-2Y-0.6Nd-0.6Zr alloy were investigated by X-ray diffraction (XRD) and electron backscattered diffraction (EBSD), after equal channel angular deformation. The results showed that after seven passes of rolling, the grain size in the Mg-2Y-0.6Nd-0.6Zr alloy was refined to approximately 22 µm and the slip occurred mainly by a cylindrical slip and a pyramidal slip. After one pass of ECAP at 340 °C, the internal average grain size was significantly reduced to 11 µm, the cylindrical diffraction intensity clearly weakened, and the pyramidal diffraction intensity increased. EBSD pole figure analysis revealed that the base texture of the rolled Mg-2Y-0.6Nd-0.6Zr alloy weakened from 24.31 to 11.34 after ECAP. The mechanical properties indicated that the tensile strength and elongation of the rolled Mg-2Y-0.6Nd-0.6Zr alloy reached maximum values, when the deformation temperature was 340 °C.
topic Mg-2Y-0.6Nd-0.6Zr alloy
equal channel angular pressing
predeformation
deformation temperature
url https://www.mdpi.com/1996-1944/12/9/1554
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