Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester

An ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dim...

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Main Author: FAN Hong-yu
Format: Article
Language:zho
Published: Science Press 2018-03-01
Series:Chinese Journal of Magnetic Resonance
Subjects:
NMR
Online Access:http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584
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spelling doaj-1d55d8b360ea4514bc2cc1cc377c09d72020-11-24T23:07:51ZzhoScience PressChinese Journal of Magnetic Resonance1000-45561000-45562018-03-013519810810.11938/cjmr20172584Spectral Analyses of a Novel Ibuprofen-Phillygenin EsterFAN Hong-yu01. Dalian Fusheng Natural Pharmaceutical Co., Ltd., Dalian 116000, China; 2. Liaoning API and Formulation of Traditional Chinese Medicine Monomer Engineering Technology Research Center, Dalian 116000, ChinaAn ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dimensional/two dimensional nuclear magnetic resonance (NMR) spectra (i.e., 1H-NMR, 13C-NMR, 13C-DEPT, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC) of the compound were collected. All 1H and 13C NMR signals were assigned.http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584NMRphillygeninibuprofeninfrared absorption spectrum (IR)ultraviolet absorption spectrum (UV)
collection DOAJ
language zho
format Article
sources DOAJ
author FAN Hong-yu
spellingShingle FAN Hong-yu
Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
Chinese Journal of Magnetic Resonance
NMR
phillygenin
ibuprofen
infrared absorption spectrum (IR)
ultraviolet absorption spectrum (UV)
author_facet FAN Hong-yu
author_sort FAN Hong-yu
title Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
title_short Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
title_full Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
title_fullStr Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
title_full_unstemmed Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
title_sort spectral analyses of a novel ibuprofen-phillygenin ester
publisher Science Press
series Chinese Journal of Magnetic Resonance
issn 1000-4556
1000-4556
publishDate 2018-03-01
description An ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dimensional/two dimensional nuclear magnetic resonance (NMR) spectra (i.e., 1H-NMR, 13C-NMR, 13C-DEPT, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC) of the compound were collected. All 1H and 13C NMR signals were assigned.
topic NMR
phillygenin
ibuprofen
infrared absorption spectrum (IR)
ultraviolet absorption spectrum (UV)
url http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584
work_keys_str_mv AT fanhongyu spectralanalysesofanovelibuprofenphillygeninester
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