Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester
An ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dim...
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Online Access: | http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584 |
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doaj-1d55d8b360ea4514bc2cc1cc377c09d72020-11-24T23:07:51ZzhoScience PressChinese Journal of Magnetic Resonance1000-45561000-45562018-03-013519810810.11938/cjmr20172584Spectral Analyses of a Novel Ibuprofen-Phillygenin EsterFAN Hong-yu01. Dalian Fusheng Natural Pharmaceutical Co., Ltd., Dalian 116000, China; 2. Liaoning API and Formulation of Traditional Chinese Medicine Monomer Engineering Technology Research Center, Dalian 116000, ChinaAn ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dimensional/two dimensional nuclear magnetic resonance (NMR) spectra (i.e., 1H-NMR, 13C-NMR, 13C-DEPT, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC) of the compound were collected. All 1H and 13C NMR signals were assigned.http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584NMRphillygeninibuprofeninfrared absorption spectrum (IR)ultraviolet absorption spectrum (UV) |
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DOAJ |
language |
zho |
format |
Article |
sources |
DOAJ |
author |
FAN Hong-yu |
spellingShingle |
FAN Hong-yu Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester Chinese Journal of Magnetic Resonance NMR phillygenin ibuprofen infrared absorption spectrum (IR) ultraviolet absorption spectrum (UV) |
author_facet |
FAN Hong-yu |
author_sort |
FAN Hong-yu |
title |
Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester |
title_short |
Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester |
title_full |
Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester |
title_fullStr |
Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester |
title_full_unstemmed |
Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester |
title_sort |
spectral analyses of a novel ibuprofen-phillygenin ester |
publisher |
Science Press |
series |
Chinese Journal of Magnetic Resonance |
issn |
1000-4556 1000-4556 |
publishDate |
2018-03-01 |
description |
An ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dimensional/two dimensional nuclear magnetic resonance (NMR) spectra (i.e., 1H-NMR, 13C-NMR, 13C-DEPT, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC) of the compound were collected. All 1H and 13C NMR signals were assigned. |
topic |
NMR phillygenin ibuprofen infrared absorption spectrum (IR) ultraviolet absorption spectrum (UV) |
url |
http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584 |
work_keys_str_mv |
AT fanhongyu spectralanalysesofanovelibuprofenphillygeninester |
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1725616675531784192 |