Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester

Spectral Analyses of a Novel Ibuprofen-Phillygenin Ester

An ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dim...

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Bibliographic Details
Main Author: FAN Hong-yu
Format: Article
Language:zho
Published: Science Press 2018-03-01
Series:Chinese Journal of Magnetic Resonance
Subjects:
NMR
phillygenin
ibuprofen
infrared absorption spectrum (IR)
ultraviolet absorption spectrum (UV)
Online Access:http://121.43.60.238/bpxzz/EN/10.11938/cjmr20172584
Description
Summary:An ibuprofen-phillygenin ester was synthesized through the Schotten-Baumann reaction with ibuprofen and phillygenin as the starting materials. Ultraviolet absorption (UV) spectrum, infrared absorption (IR) spectrum, matrix-assisted laser desorption/ionization-mass spectra (MALDI-TOF-MS), and one-dimensional/two dimensional nuclear magnetic resonance (NMR) spectra (i.e., 1H-NMR, 13C-NMR, 13C-DEPT, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC) of the compound were collected. All 1H and 13C NMR signals were assigned.
ISSN:1000-4556
1000-4556

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