Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O

Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O

C33H34N5O3Br, triclinic, P1̄ (no. 2), a = 9.1179(2) Å, b = 9.3291(3) Å, c = 18.4706(6) Å, α = 91.187(3)°, β = 95.764(2)°, γ = 102.256(2)°, Z = 2, V = 1526.15(8) Å3, Rgt(F) = 0.0357, wRref(F2) = 0.0954, T = 105.7(5) K.

Bibliographic Details
Main Authors: Xing Ai-Ping, Zeng Dai
Format: Article
Language:English
Published: De Gruyter 2019-06-01
Series:Zeitschrift für Kristallographie - New Crystal Structures
Subjects:
1892532
Online Access:https://doi.org/10.1515/ncrs-2018-0500
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spelling doaj-1d0a9e67eb1741b483869341167169762021-09-06T19:20:56ZengDe GruyterZeitschrift für Kristallographie - New Crystal Structures1433-72662197-45782019-06-01234459960110.1515/ncrs-2018-0500Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4OXing Ai-Ping0Zeng Dai1Henan University of Chinese Medicine, Zhengzhou 450046, P.R. ChinaHenan University of Chinese Medicine, Zhengzhou 450046, P.R. ChinaC33H34N5O3Br, triclinic, P1̄ (no. 2), a = 9.1179(2) Å, b = 9.3291(3) Å, c = 18.4706(6) Å, α = 91.187(3)°, β = 95.764(2)°, γ = 102.256(2)°, Z = 2, V = 1526.15(8) Å3, Rgt(F) = 0.0357, wRref(F2) = 0.0954, T = 105.7(5) K.https://doi.org/10.1515/ncrs-2018-05001892532
collection DOAJ
language English
format Article
sources DOAJ
author Xing Ai-Ping
Zeng Dai
spellingShingle Xing Ai-Ping
Zeng Dai
Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O
Zeitschrift für Kristallographie - New Crystal Structures
1892532
author_facet Xing Ai-Ping
Zeng Dai
author_sort Xing Ai-Ping
title Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O
title_short Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O
title_full Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O
title_fullStr Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O
title_full_unstemmed Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C32H30N5O2Br ⋅ CH4O
title_sort crystal structure of (e)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), c32h30n5o2br ⋅ ch4o
publisher De Gruyter
series Zeitschrift für Kristallographie - New Crystal Structures
issn 1433-7266
2197-4578
publishDate 2019-06-01
description C33H34N5O3Br, triclinic, P1̄ (no. 2), a = 9.1179(2) Å, b = 9.3291(3) Å, c = 18.4706(6) Å, α = 91.187(3)°, β = 95.764(2)°, γ = 102.256(2)°, Z = 2, V = 1526.15(8) Å3, Rgt(F) = 0.0357, wRref(F2) = 0.0954, T = 105.7(5) K.
topic 1892532
url https://doi.org/10.1515/ncrs-2018-0500
work_keys_str_mv AT xingaiping crystalstructureofe26bromopyridin2ylmethyleneamino36bisethylamino27dimethylspiroisoindoline19xanthen3onemethanol11c32h30n5o2brch4o
AT zengdai crystalstructureofe26bromopyridin2ylmethyleneamino36bisethylamino27dimethylspiroisoindoline19xanthen3onemethanol11c32h30n5o2brch4o
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