Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method
A facile low temperature co-precipitation method for the synthesis of crystalline cobalt ferrite nanostructures using ferrous sulfate salt as the precursor has been discussed. The prepared samples were compared with nanoparticles prepared by conventional co-precipitation and hydrothermal methods usi...
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doaj-1cf2f7dca74d4b0c8e6dce8d53eb19a72020-11-25T01:01:09ZengAIP Publishing LLCAIP Advances2158-32262016-05-0165055904055904-710.1063/1.4942951023691ADVMagnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based methodTejabhiram Yadavalli0Hardik Jain1Gopalakrishnan Chandrasekharan2Ramasamy Chennakesavulu3Nanotechnology Research Center, SRM University, SRM Nagar, Kattankulathur, Kancheepuram Dist, Tamilnadu, India – 603203Department of Physics and Nanotechnology, SRM University, SRM Nagar, Kattankulathur, Kancheepuram Dist, Tamilnadu, India – 603203Nanotechnology Research Center, SRM University, SRM Nagar, Kattankulathur, Kancheepuram Dist, Tamilnadu, India – 603203Department of Pharmacy Practice, SRM University, SRM Nagar, Kattankulathur, Kancheepuram Dist, Tamilnadu, India – 603203A facile low temperature co-precipitation method for the synthesis of crystalline cobalt ferrite nanostructures using ferrous sulfate salt as the precursor has been discussed. The prepared samples were compared with nanoparticles prepared by conventional co-precipitation and hydrothermal methods using ferric nitrate as the precursor. X-ray diffraction studies confirmed the formation of cubic spinel cobalt ferrites when dried at 110 °C as opposed to conventional methods which required higher temperatures/pressure for the formation of the same. Field emission scanning electron microscope studies of these powders revealed the formation of nearly spherical nanostructures in the size range of 20-30 nm which were comparable to those prepared by conventional methods. Magnetic measurements confirmed the ferromagnetic nature of the cobalt ferrites with low magnetic remanance. Further magnetic hyperthermia studies of nanostructures prepared by low temperature method showed a rise in temperature to 50 °C in 600 s.http://dx.doi.org/10.1063/1.4942951 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Tejabhiram Yadavalli Hardik Jain Gopalakrishnan Chandrasekharan Ramasamy Chennakesavulu |
spellingShingle |
Tejabhiram Yadavalli Hardik Jain Gopalakrishnan Chandrasekharan Ramasamy Chennakesavulu Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method AIP Advances |
author_facet |
Tejabhiram Yadavalli Hardik Jain Gopalakrishnan Chandrasekharan Ramasamy Chennakesavulu |
author_sort |
Tejabhiram Yadavalli |
title |
Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method |
title_short |
Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method |
title_full |
Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method |
title_fullStr |
Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method |
title_full_unstemmed |
Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method |
title_sort |
magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method |
publisher |
AIP Publishing LLC |
series |
AIP Advances |
issn |
2158-3226 |
publishDate |
2016-05-01 |
description |
A facile low temperature co-precipitation method for the synthesis of crystalline cobalt ferrite nanostructures using ferrous sulfate salt as the precursor has been discussed. The prepared samples were compared with nanoparticles prepared by conventional co-precipitation and hydrothermal methods using ferric nitrate as the precursor. X-ray diffraction studies confirmed the formation of cubic spinel cobalt ferrites when dried at 110 °C as opposed to conventional methods which required higher temperatures/pressure for the formation of the same. Field emission scanning electron microscope studies of these powders revealed the formation of nearly spherical nanostructures in the size range of 20-30 nm which were comparable to those prepared by conventional methods. Magnetic measurements confirmed the ferromagnetic nature of the cobalt ferrites with low magnetic remanance. Further magnetic hyperthermia studies of nanostructures prepared by low temperature method showed a rise in temperature to 50 °C in 600 s. |
url |
http://dx.doi.org/10.1063/1.4942951 |
work_keys_str_mv |
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