Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy

This article describes the successful application of the DOSY method for the separation and analysis of the α- and β-anomers of carbohydrates with different diffusion coefficients. In addition, the DOSY method was found to effectively separate two kinds of glucopyranosides with similar aglycon struc...

Full description

Bibliographic Details
Main Authors:	Takashi Yamanoi, Yoshiki Oda, Kaname Katsuraya
Format:	Article
Language:	English
Published:	MDPI AG 2017-11-01
Series:	Magnetochemistry
Subjects:	DOSY diffusion coefficient anomer separation carbohydrate isomer glycoside
Online Access:	https://www.mdpi.com/2312-7481/3/4/38

id	doaj-1b803cb56f8e471eaa174ba486a83c8a
record_format	Article
spelling	doaj-1b803cb56f8e471eaa174ba486a83c8a2020-11-25T02:43:09ZengMDPI AGMagnetochemistry2312-74812017-11-01343810.3390/magnetochemistry3040038magnetochemistry3040038Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR SpectroscopyTakashi Yamanoi0Yoshiki Oda1Kaname Katsuraya2Faculty of Pharmacy and Pharmaceutical Sciences, Josai University, 1-1 Keyakidai, Sakado, Saitama 350-0295, JapanTechnology Joint Management Office, Tokai University, 4-1-1 Kitakaname, Hiratsuka, Kanagawa 259-1292, JapanDepartment of Human Ecology, Wayo Women’s University, Chiba 272-8533, JapanThis article describes the successful application of the DOSY method for the separation and analysis of the α- and β-anomers of carbohydrates with different diffusion coefficients. In addition, the DOSY method was found to effectively separate two kinds of glucopyranosides with similar aglycon structures from a mixture.https://www.mdpi.com/2312-7481/3/4/38DOSYdiffusion coefficientanomer separationcarbohydrate isomerglycoside
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Takashi Yamanoi Yoshiki Oda Kaname Katsuraya
spellingShingle	Takashi Yamanoi Yoshiki Oda Kaname Katsuraya Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy Magnetochemistry DOSY diffusion coefficient anomer separation carbohydrate isomer glycoside
author_facet	Takashi Yamanoi Yoshiki Oda Kaname Katsuraya
author_sort	Takashi Yamanoi
title	Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy
title_short	Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy
title_full	Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy
title_fullStr	Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy
title_full_unstemmed	Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy
title_sort	separation of the α- and β-anomers of carbohydrates by diffusion-ordered nmr spectroscopy
publisher	MDPI AG
series	Magnetochemistry
issn	2312-7481
publishDate	2017-11-01
description	This article describes the successful application of the DOSY method for the separation and analysis of the α- and β-anomers of carbohydrates with different diffusion coefficients. In addition, the DOSY method was found to effectively separate two kinds of glucopyranosides with similar aglycon structures from a mixture.
topic	DOSY diffusion coefficient anomer separation carbohydrate isomer glycoside
url	https://www.mdpi.com/2312-7481/3/4/38
work_keys_str_mv	AT takashiyamanoi separationoftheaandbanomersofcarbohydratesbydiffusionorderednmrspectroscopy AT yoshikioda separationoftheaandbanomersofcarbohydratesbydiffusionorderednmrspectroscopy AT kanamekatsuraya separationoftheaandbanomersofcarbohydratesbydiffusionorderednmrspectroscopy
_version_	1724771152910352384

Separation of the α- and β-Anomers of Carbohydrates by Diffusion-Ordered NMR Spectroscopy

Similar Items