The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide

The structure of the title quinoline carboxamide derivative, C26H25N3O, is described. The quinoline moiety is not planar as a result of a slight puckering of the pyridine ring. The secondary amine has a slightly pyramidal geometry, certainly not planar. Both intra- and intermolecular hydrogen bonds...

Full description

Bibliographic Details
Main Authors:	Ligia R. Gomes, John Nicolson Low, Fernanda Borges, Alexandra Gaspar, Francesco Mesiti
Format:	Article
Language:	English
Published:	International Union of Crystallography 2020-02-01
Series:	Acta Crystallographica Section E: Crystallographic Communications
Subjects:	crystal structure hydrogen bonding quinoline carboxamide amine
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2056989020000298

id	doaj-1a89401935584386bd1408bb090de751
record_format	Article
spelling	doaj-1a89401935584386bd1408bb090de7512020-11-25T00:26:58ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902020-02-0176220120710.1107/S2056989020000298zl2767The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamideLigia R. Gomes0John Nicolson Low1Fernanda Borges2Alexandra Gaspar3Francesco Mesiti4REQUIMTE, Departamento de Química e Bioquímica, Faculdade de Ciências da Universidade do Porto, Rua do Campo Alegre, 687, P-4169-007, Porto, PortugalDepartment of Chemistry, University of Aberdeen, Meston Walk, Old Aberdeen, AB24 3UE, ScotlandCIQUP Departamento de Quιmica e Bioquιmica, Faculdade de Ciências, Universidade do Porto, 4169-007 Porto, PortugalCIQUP Departamento de Quιmica e Bioquιmica, Faculdade de Ciências, Universidade do Porto, 4169-007 Porto, PortugalDepartment of "Scienze della Vita", University "Magna Graecia" of Catanzaro, Catanzaro, ItalyThe structure of the title quinoline carboxamide derivative, C26H25N3O, is described. The quinoline moiety is not planar as a result of a slight puckering of the pyridine ring. The secondary amine has a slightly pyramidal geometry, certainly not planar. Both intra- and intermolecular hydrogen bonds are present. Hirshfeld surface analysis and lattice energies were used to investigate the intermolecular interactions.http://scripts.iucr.org/cgi-bin/paper?S2056989020000298crystal structurehydrogen bondingquinolinecarboxamideamine
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Ligia R. Gomes John Nicolson Low Fernanda Borges Alexandra Gaspar Francesco Mesiti
spellingShingle	Ligia R. Gomes John Nicolson Low Fernanda Borges Alexandra Gaspar Francesco Mesiti The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide Acta Crystallographica Section E: Crystallographic Communications crystal structure hydrogen bonding quinoline carboxamide amine
author_facet	Ligia R. Gomes John Nicolson Low Fernanda Borges Alexandra Gaspar Francesco Mesiti
author_sort	Ligia R. Gomes
title	The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide
title_short	The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide
title_full	The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide
title_fullStr	The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide
title_full_unstemmed	The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide
title_sort	synthesis, crystal structure and hirshfeld analysis of 4-(3,4-dimethylanilino)-n-(3,4-dimethylphenyl)quinoline-3-carboxamide
publisher	International Union of Crystallography
series	Acta Crystallographica Section E: Crystallographic Communications
issn	2056-9890
publishDate	2020-02-01
description	The structure of the title quinoline carboxamide derivative, C26H25N3O, is described. The quinoline moiety is not planar as a result of a slight puckering of the pyridine ring. The secondary amine has a slightly pyramidal geometry, certainly not planar. Both intra- and intermolecular hydrogen bonds are present. Hirshfeld surface analysis and lattice energies were used to investigate the intermolecular interactions.
topic	crystal structure hydrogen bonding quinoline carboxamide amine
url	http://scripts.iucr.org/cgi-bin/paper?S2056989020000298
work_keys_str_mv	AT ligiargomes thesynthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT johnnicolsonlow thesynthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT fernandaborges thesynthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT alexandragaspar thesynthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT francescomesiti thesynthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT ligiargomes synthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT johnnicolsonlow synthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT fernandaborges synthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT alexandragaspar synthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide AT francescomesiti synthesiscrystalstructureandhirshfeldanalysisof434dimethylanilinon34dimethylphenylquinoline3carboxamide
_version_	1725341713729323008

The synthesis, crystal structure and Hirshfeld analysis of 4-(3,4-dimethylanilino)-N-(3,4-dimethylphenyl)quinoline-3-carboxamide

Similar Items