1,2,3,4-Tetra-O-Acetyl-β-d-Mannuronic Acid

1,2,3,4-Tetra-O-acetyl-β-d-mannuronic acid was synthesized in three steps from commercial d-mannose in 21% yield. Regioselective 6-O-tritylation followed by per-acetylation and 6-OTr removal using HBr/AcOH gave the required primary alcohol substrate, which was then oxidised to the target compound us...

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Bibliographic Details
Main Authors: Laura Beswick, Gavin J. Miller
Format: Article
Language:English
Published: MDPI AG 2017-07-01
Series:Molbank
Subjects:
NMR
Online Access:https://www.mdpi.com/1422-8599/2017/3/M947