The synthesis and characterization of 2-mercaptoethyl methacrylate

The synthesis of 2-mercaptoethyl methacrylate from methacrylic acid and 2-mercaptoethanol by etherification using acetyl chloride as catalyst was optimized. The purity of the obtained product was controlled by gas chromatography and its identity confirmed by H-NMR and FTIR spectroscopy. 2-Mercapto-e...

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Bibliographic Details
Main Authors: Knežević Marija, Katsikas Lynne, Popović Ivanka G.
Format: Article
Language:English
Published: Association of Chemical Engineers of Serbia 2005-01-01
Series:Hemijska Industrija
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/0367-598X/2005/0367-598X0512321K.pdf
Description
Summary:The synthesis of 2-mercaptoethyl methacrylate from methacrylic acid and 2-mercaptoethanol by etherification using acetyl chloride as catalyst was optimized. The purity of the obtained product was controlled by gas chromatography and its identity confirmed by H-NMR and FTIR spectroscopy. 2-Mercapto-ethyl methacrylate could find application as a chain transfer agent in radical polymerizations.
ISSN:0367-598X