Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads

With the characteristics of gradual instability in the supporting pressure area of roadway as the engineering background, this paper aims to explore the evolution law of pore and fracture in the coal sample under progressive loads. The low-field nuclear magnetic resonance (NMR) test was designed and...

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Main Authors: Zhengzheng Xie, Nong Zhang, Jin Wang, Zhe Xiang, Chenghao Zhang
Format: Article
Language:English
Published: MDPI AG 2020-09-01
Series:Applied Sciences
Subjects:
NMR
MRI
Online Access:https://www.mdpi.com/2076-3417/10/18/6526
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spelling doaj-17a4ec4a93fd48b088ff99b44b5655442020-11-25T03:43:30ZengMDPI AGApplied Sciences2076-34172020-09-01106526652610.3390/app10186526Study on Magnetic Resonance Characteristics of Coal Sample under Progressive LoadsZhengzheng Xie0Nong Zhang1Jin Wang2Zhe Xiang3Chenghao Zhang4Key Laboratory of Deep Coal Resource Mining, Ministry of Education of China, School of Mines, China University of Mining and Technology, Xuzhou 221116, Jiangsu, ChinaKey Laboratory of Deep Coal Resource Mining, Ministry of Education of China, School of Mines, China University of Mining and Technology, Xuzhou 221116, Jiangsu, ChinaKey Laboratory of Deep Coal Resource Mining, Ministry of Education of China, School of Mines, China University of Mining and Technology, Xuzhou 221116, Jiangsu, ChinaKey Laboratory of Deep Coal Resource Mining, Ministry of Education of China, School of Mines, China University of Mining and Technology, Xuzhou 221116, Jiangsu, ChinaLaboratory of Geotechnics, Department of Civil Engineering, Ghent University, Zwijnaarde, 9052 Gent, BelgiumWith the characteristics of gradual instability in the supporting pressure area of roadway as the engineering background, this paper aims to explore the evolution law of pore and fracture in the coal sample under progressive loads. The low-field nuclear magnetic resonance (NMR) test was designed and conducted with the coal sample under different axial loads (0, 3, 5, 7, 9, and 11 MPa). The characteristic parameters such as the porosity, the pore size distribution, the transverse relaxation time (<i>T</i><sub>2</sub>) distribution curve, and the magnetic resonance image (MRI) were obtained. As the test results show, significant difference in the NMR characteristics of the coal samples can be observed throughout the compaction stage and the elastic stage. In the compaction stage, the porosity of the coal samples decreases slightly; the <i>T</i><sub>2</sub> distribution curve moves to the smaller value as a whole, and the percolation pore (PP) displays a tendency to transform to the adsorption pore (AP). In the elastic stage, the porosity of the coal samples rises gradually as the load increases; the <i>T</i><sub>2</sub> distribution curve moves to the larger value as a whole, and the AP tends to transform to the PP. The MRI shows that some pores and fissures in the coal sample close up and disappear as the load increases gradually, while the main pores and fissures expand and perforate till the macro failure occurs. Compared with one-time loading, the progressive multiple loads can ensure the fracture of the coal sample to develop more fully and the damage degree higher. It indirectly reflects that the instability and failure of the coal under the progressive load has the stage characteristics, verifying that the coal in the supporting pressure area needs to be controlled in advance.https://www.mdpi.com/2076-3417/10/18/6526coal sampleNMRprogressive loadporosityfissure propagationMRI
collection DOAJ
language English
format Article
sources DOAJ
author Zhengzheng Xie
Nong Zhang
Jin Wang
Zhe Xiang
Chenghao Zhang
spellingShingle Zhengzheng Xie
Nong Zhang
Jin Wang
Zhe Xiang
Chenghao Zhang
Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads
Applied Sciences
coal sample
NMR
progressive load
porosity
fissure propagation
MRI
author_facet Zhengzheng Xie
Nong Zhang
Jin Wang
Zhe Xiang
Chenghao Zhang
author_sort Zhengzheng Xie
title Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads
title_short Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads
title_full Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads
title_fullStr Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads
title_full_unstemmed Study on Magnetic Resonance Characteristics of Coal Sample under Progressive Loads
title_sort study on magnetic resonance characteristics of coal sample under progressive loads
publisher MDPI AG
series Applied Sciences
issn 2076-3417
publishDate 2020-09-01
description With the characteristics of gradual instability in the supporting pressure area of roadway as the engineering background, this paper aims to explore the evolution law of pore and fracture in the coal sample under progressive loads. The low-field nuclear magnetic resonance (NMR) test was designed and conducted with the coal sample under different axial loads (0, 3, 5, 7, 9, and 11 MPa). The characteristic parameters such as the porosity, the pore size distribution, the transverse relaxation time (<i>T</i><sub>2</sub>) distribution curve, and the magnetic resonance image (MRI) were obtained. As the test results show, significant difference in the NMR characteristics of the coal samples can be observed throughout the compaction stage and the elastic stage. In the compaction stage, the porosity of the coal samples decreases slightly; the <i>T</i><sub>2</sub> distribution curve moves to the smaller value as a whole, and the percolation pore (PP) displays a tendency to transform to the adsorption pore (AP). In the elastic stage, the porosity of the coal samples rises gradually as the load increases; the <i>T</i><sub>2</sub> distribution curve moves to the larger value as a whole, and the AP tends to transform to the PP. The MRI shows that some pores and fissures in the coal sample close up and disappear as the load increases gradually, while the main pores and fissures expand and perforate till the macro failure occurs. Compared with one-time loading, the progressive multiple loads can ensure the fracture of the coal sample to develop more fully and the damage degree higher. It indirectly reflects that the instability and failure of the coal under the progressive load has the stage characteristics, verifying that the coal in the supporting pressure area needs to be controlled in advance.
topic coal sample
NMR
progressive load
porosity
fissure propagation
MRI
url https://www.mdpi.com/2076-3417/10/18/6526
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AT jinwang studyonmagneticresonancecharacteristicsofcoalsampleunderprogressiveloads
AT zhexiang studyonmagneticresonancecharacteristicsofcoalsampleunderprogressiveloads
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