Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa2Cu3O7−δ Superconductor: Effect of Addition of SnO2 Nanoparticles

YBa2Cu3O7−δ (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO2 nanoparticles were synthesised via a thermal treatment method. The influence of SnO2 addition on the superconducting properties by means of critical temperature, Tc, AC susc...

Full description

Bibliographic Details
Main Authors: Nur Nabilah Mohd Yusuf, Mohd Mustafa Awang Kechik, Hussein Baqiah, Chen Soo Kien, Lim Kean Pah, Abdul Halim Shaari, Wan Nur Wathiq Wan Jusoh, Safia Izzati Abd Sukor, Mustafa Mousa Dihom, Zainal Abidin Talib, Roslan Abd-Shukor
Format: Article
Language:English
Published: MDPI AG 2018-12-01
Series:Materials
Subjects:
Online Access:http://www.mdpi.com/1996-1944/12/1/92
Description
Summary:YBa2Cu3O7−δ (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO2 nanoparticles were synthesised via a thermal treatment method. The influence of SnO2 addition on the superconducting properties by means of critical temperature, Tc, AC susceptibility, phase formation and microstructures, including its elemental composition analysis, were studied. Sharp superconducting transition, ∆Tc, and diamagnetic transition were obtained for all SnO2-added samples. It was observed that sample x = 0.4 with a Y-123 phase percentage of 95.8% gives the highest Tc, smallest ∆Tc, and the sharpest diamagnetic transition in the normalised susceptibility curves. The microstructure also showed an excess of Sn precipitates on the sample’s surface at x = 0.8 and above. As such, the best superconducting properties were observed at x = 0.4 SnO2 addition inside the Y-123 host sample.
ISSN:1996-1944