(E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate

(E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate

In the title compound, C14H9Br2N3O4·CH3OH, the Schiff base molecule adopts an E geometry with respect to the C=N bond and the benzene rings are oriented at a dihedral angle of 45.3 (2)°. An intramolecular O—H...N hydrogen bond helps to establish...

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Main Authors: Heng-Yu Qian, Da-Ping Qu
Format: Article
Language:English
Published: International Union of Crystallography 2009-09-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S160053680903311X
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spelling doaj-17310675597d498d9e84371702613b802020-11-24T22:09:23ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-09-01659o2237o223710.1107/S160053680903311X(E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvateHeng-Yu QianDa-Ping QuIn the title compound, C14H9Br2N3O4·CH3OH, the Schiff base molecule adopts an E geometry with respect to the C=N bond and the benzene rings are oriented at a dihedral angle of 45.3 (2)°. An intramolecular O—H...N hydrogen bond helps to establish the conformation. In the crystal, the methanol solvent molecule is linked to the Schiff base molecule through an O—H...O hydrogen bond and intermolecular N—H...O hydrogen bonds link the components to form layers parallel to the bc direction. http://scripts.iucr.org/cgi-bin/paper?S160053680903311X
collection DOAJ
language English
format Article
sources DOAJ
author Heng-Yu Qian
Da-Ping Qu
spellingShingle Heng-Yu Qian
Da-Ping Qu
(E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
Acta Crystallographica Section E
author_facet Heng-Yu Qian
Da-Ping Qu
author_sort Heng-Yu Qian
title (E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
title_short (E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
title_full (E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
title_fullStr (E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
title_full_unstemmed (E)-N′-(3,5-Dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
title_sort (e)-n′-(3,5-dibromo-2-hydroxybenzylidene)-2-nitrobenzohydrazide methanol solvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-09-01
description In the title compound, C14H9Br2N3O4·CH3OH, the Schiff base molecule adopts an E geometry with respect to the C=N bond and the benzene rings are oriented at a dihedral angle of 45.3 (2)°. An intramolecular O—H...N hydrogen bond helps to establish the conformation. In the crystal, the methanol solvent molecule is linked to the Schiff base molecule through an O—H...O hydrogen bond and intermolecular N—H...O hydrogen bonds link the components to form layers parallel to the bc direction.
url http://scripts.iucr.org/cgi-bin/paper?S160053680903311X
work_keys_str_mv AT hengyuqian enamp824235dibromo2hydroxybenzylidene2nitrobenzohydrazidemethanolsolvate
AT dapingqu enamp824235dibromo2hydroxybenzylidene2nitrobenzohydrazidemethanolsolvate
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