2-(5-Iodo-2-oxoindolin-3-ylidene)hydrazinecarbothioamide including an unknown solvate

The molecule of the title compound, C9H7IN4OS, is almost planar (r.m.s. deviation = 0.0373 Å). In the molecule, N—H...N and N—H...O hydrogen bonds generate, respectively, S(5) and S(6) ring motifs. In the crystal, molecules are linked via N—H...O hydrogen bonds, forming chains propagating along [010...

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Bibliographic Details
Main Authors: Viviane Conceição Duarte de Bittencourt, Vanessa Carratu Gervini, Juliano Rosa de Menezes Vicenti, Jecika Maciel Velasques, Priscilla Jussiane Zambiazi
Format: Article
Language:English
Published: International Union of Crystallography 2014-06-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536814010782
Description
Summary:The molecule of the title compound, C9H7IN4OS, is almost planar (r.m.s. deviation = 0.0373 Å). In the molecule, N—H...N and N—H...O hydrogen bonds generate, respectively, S(5) and S(6) ring motifs. In the crystal, molecules are linked via N—H...O hydrogen bonds, forming chains propagating along [010]. These chains are linked via S...I contacts [3.4915 (16) Å], forming sheets lying parallel to (100). A region of disordered electron density, probably a disordered tetrahydrofuran solvent molecule, was treated using the SQUEEZE routine in PLATON [Spek (2009). Acta Cryst. D65, 148–155]. The formula mass and unit-cell characteristics were not taken into account during refinement.
ISSN:1600-5368