2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide
The title compound, 2-methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl) ethenyl-3, 4-dihydroquinazolin-3-yl] benzene-1-sulfonamide <strong>2</strong> has been synthesized by the reaction of 3-(4-methoxyphenyl)-2-styryl-4(3<em>...
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Online Access: | http://www.mdpi.com/1422-8599/2012/3/M765 |
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doaj-11f56f471009462082b704d0ad467b832020-11-24T21:51:06ZengMDPI AGMolbank1422-85992012-07-0120123M76510.3390/M7652-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamideSumi HudiyonoHayunArry YanuarMuhammad HanafiThe title compound, 2-methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl) ethenyl-3, 4-dihydroquinazolin-3-yl] benzene-1-sulfonamide <strong>2</strong> has been synthesized by the reaction of 3-(4-methoxyphenyl)-2-styryl-4(3<em>H</em>)-quinazolinone <strong>1</strong> with an excess of chlorosulfonic acid, followed by amidation of the sulfonyl chloride product with ammonia gas. The structure of the synthesized compound was confirmed on the basis of IR, <sup>1</sup>H-NMR, <sup>13</sup>C-NMR and mass spectral data.http://www.mdpi.com/1422-8599/2012/3/M7654(3<em>H</em>)-quinazolinone2-styryl-4(3<em>H</em>)-quinazolinonebenzenesulfonamidechlorosulfonation-amidation |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Sumi Hudiyono Hayun Arry Yanuar Muhammad Hanafi |
spellingShingle |
Sumi Hudiyono Hayun Arry Yanuar Muhammad Hanafi 2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide Molbank 4(3<em>H</em>)-quinazolinone 2-styryl-4(3<em>H</em>)-quinazolinone benzenesulfonamide chlorosulfonation-amidation |
author_facet |
Sumi Hudiyono Hayun Arry Yanuar Muhammad Hanafi |
author_sort |
Sumi Hudiyono |
title |
2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide |
title_short |
2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide |
title_full |
2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide |
title_fullStr |
2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide |
title_full_unstemmed |
2-Methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide |
title_sort |
2-methoxy-5-{4-oxo-2-[(<em>e</em>)-2-(4-sulfamoylphenyl)ethenyl-3,4-dihydroquinazolin-3-yl]benzene-1-sulfonamide |
publisher |
MDPI AG |
series |
Molbank |
issn |
1422-8599 |
publishDate |
2012-07-01 |
description |
The title compound, 2-methoxy-5-{4-oxo-2-[(<em>E</em>)-2-(4-sulfamoylphenyl) ethenyl-3, 4-dihydroquinazolin-3-yl] benzene-1-sulfonamide <strong>2</strong> has been synthesized by the reaction of 3-(4-methoxyphenyl)-2-styryl-4(3<em>H</em>)-quinazolinone <strong>1</strong> with an excess of chlorosulfonic acid, followed by amidation of the sulfonyl chloride product with ammonia gas. The structure of the synthesized compound was confirmed on the basis of IR, <sup>1</sup>H-NMR, <sup>13</sup>C-NMR and mass spectral data. |
topic |
4(3<em>H</em>)-quinazolinone 2-styryl-4(3<em>H</em>)-quinazolinone benzenesulfonamide chlorosulfonation-amidation |
url |
http://www.mdpi.com/1422-8599/2012/3/M765 |
work_keys_str_mv |
AT sumihudiyono 2methoxy54oxo2ltemgteltemgt24sulfamoylphenylethenyl34dihydroquinazolin3ylbenzene1sulfonamide AT hayun 2methoxy54oxo2ltemgteltemgt24sulfamoylphenylethenyl34dihydroquinazolin3ylbenzene1sulfonamide AT arryyanuar 2methoxy54oxo2ltemgteltemgt24sulfamoylphenylethenyl34dihydroquinazolin3ylbenzene1sulfonamide AT muhammadhanafi 2methoxy54oxo2ltemgteltemgt24sulfamoylphenylethenyl34dihydroquinazolin3ylbenzene1sulfonamide |
_version_ |
1725880450737504256 |