Unambiguous Ex Situ and in Cell 2D <sup>13</sup>C Solid-State NMR Characterization of Starch and Its Constituents

Unambiguous Ex Situ and in Cell 2D <sup>13</sup>C Solid-State NMR Characterization of Starch and Its Constituents

Starch is the most abundant energy storage molecule in plants and is an essential part of the human diet. This glucose polymer is composed of amorphous and crystalline domains in different forms (A and B types) with specific physicochemical properties that determine its bioavailability for an organi...

Full description

Bibliographic Details
Main Authors:	Alexandre Poulhazan, Alexandre A. Arnold, Dror E. Warschawski, Isabelle Marcotte
Format:	Article
Language:	English
Published:	MDPI AG 2018-11-01
Series:	International Journal of Molecular Sciences
Subjects:	whole cell NMR magic-angle spinning 2D INADEQUATE crystalline and amorphous starch
Online Access:	https://www.mdpi.com/1422-0067/19/12/3817

Similar Items

Stochastic Modelling of <sup>13</sup>C NMR Spin Relaxation Experiments in Oligosaccharides
by: Sergio Rampino, et al.
Published: (2021-04-01)

Changes in the Crystallinity Degree of Starch Having Different Types of Crystal Structure after Mechanical Pretreatment
by: Karina Dome, et al.
Published: (2020-03-01)

Molecular Characterization of the Organic Fraction of Municipal Solid Waste and Compositional Evolution during Oxidative Processes Assessed by HR-MAS <sup>13</sup>C NMR Spectroscopy
by: Rosachiara A. Salvino, et al.
Published: (2021-03-01)

Comparison of Three Methods to Determine the Degree of Substitution of Quinoa and Rice Starch Acetates, Propionates, and Butyrates: Direct Stoichiometry, FTIR, and <sup>1</sup>H-NMR
by: Nabilah Abdul Hadi, et al.
Published: (2020-01-01)

Current Developments in µMAS NMR Analysis for Metabolomics
by: Covadonga Lucas-Torres, et al.
Published: (2019-02-01)

Solid-State <sup>2</sup>H NMR Study for Deuterated Phenylene Dynamics in a Crystalline Gyroscope-Like Molecule
by: Wataru Setaka, et al.
Published: (2021-01-01)

General Guidelines for Sample Preparation Strategies in HR-µMAS NMR-based Metabolomics of Microscopic Specimens
by: Covadonga Lucas-Torres, et al.
Published: (2020-01-01)

固体高分解能NMR　Magic Angle Spinning 法の高度化
by: 松永, 達弥
Published: (2017)

Solid-State NMR Studies of Polymeric and Biomembranes
by: Spano, Justin
Published: (2014)

Varying amylose contents affect the structural and physicochemical characteristics of starch in mung bean
by: Nguyen Thi Mai Huong, et al.
Published: (2021-01-01)

New methodologies in solid state NMR
by: Crockford, Charles
Published: (2002)

New Theoretical Approaches for Solid-State NMR of Quadrupolar Nuclei with Applications to Glass Structure
by: Trease, Nicole Marie
Published: (2009)

Ligand Control of <sup>59</sup>Co Nuclear Spin Relaxation Thermometry
by: Tyler M. Ozvat, et al.
Published: (2020-11-01)

Multiple-quantum MAS NMR of half-integer quadrupolar nuclei
by: Brown, Steven Paul
Published: (1997)

Structural Investigations of Complex Glasses by Solid-state NMR
by: Leonova, Ekaterina
Published: (2009)

Study of Liquid Crystals Showing Two Isotropic Phases by <sup>1</sup>H NMR Diffusometry and <sup>1</sup>H NMR Relaxometry
by: Anton Gradišek, et al.
Published: (2019-03-01)

Concerted suppression of all starch branching enzyme genes in barley produces amylose-only starch granules
by: Carciofi Massimiliano, et al.
Published: (2012-11-01)

Automatic 1D <sup>1</sup>H NMR Metabolite Quantification for Bioreactor Monitoring
by: Roy Chih Chung Wang, et al.
Published: (2021-03-01)

In-Cell NMR Spectroscopy: Biomolecular Structure and Function
Published: (2020)

Study of the Reactivity of Lignin Model Compounds to Fluorobenzylation Using <sup>13</sup>C and <sup>19</sup>F NMR: Application to Lignin Phenolic Hydroxyl Group Quantification by <sup>19</sup>F NMR
by: Esakkiammal Sudha Esakkimuthu, et al.
Published: (2020-07-01)

Integration of Cell-Free Expression and Solid-State NMR to Investigate the Dynamic Properties of Different Sites of the Growth Hormone Secretagogue Receptor
by: Emelyne M. Pacull, et al.
Published: (2020-10-01)

Non-Exponential <sup>1</sup>H and <sup>2</sup>H NMR Relaxation and Self-Diffusion in Asphaltene-Maltene Solutions
by: Kevin Lindt, et al.
Published: (2021-08-01)

The structural characteristics of starches and their functional properties
by: Yaeel Isbeth Cornejo-Ramírez, et al.
Published: (2018-01-01)

Effect of Initial Conformation on the Starch Biopolymer Film Formation Studied by NMR
by: Sushanta Ghoshal, et al.
Published: (2020-03-01)

Proton Detected Solid-State NMR of Membrane Proteins at 28 Tesla (1.2 GHz) and 100 kHz Magic-Angle Spinning
by: Evgeny Nimerovsky, et al.
Published: (2021-05-01)

Application of <sup>1</sup>H and <sup>13</sup>C NMR Fingerprinting as a Tool for the Authentication of Maltese Extra Virgin Olive Oil
by: Frederick Lia, et al.
Published: (2020-05-01)

Local Electronic Structure in AlN Studied by Single-Crystal <sup>27</sup>Al and <sup>14</sup>N NMR and DFT Calculations
by: Otto E. O. Zeman, et al.
Published: (2020-01-01)

Hyperpolarised <sup>1</sup>H–<sup>13</sup>C Benchtop NMR Spectroscopy
by: Alastair D. Robinson, et al.
Published: (2019-03-01)

Crosslinked Carboxymethyl Sago Starch/Citric Acid Hydrogel for Sorption of Pb<sup>2+</sup>, Cu<sup>2+</sup>, Ni<sup>2+</sup> and Zn<sup>2+</sup> from Aqueous Solution
by: Amyrah Auni Keirudin, et al.
Published: (2020-10-01)

Use of the 2D <sup>1</sup>H-<sup>13</sup>C HSQC NMR Methyl Region to Evaluate the Higher Order Structural Integrity of Biopharmaceuticals
by: Tsang-Lin Hwang, et al.
Published: (2021-05-01)

Straightforward Immobilization of Phosphonic Acids and Phosphoric Acid Esters on Mesoporous Silica and Their Application in an Asymmetric Aldol Reaction
by: Christian Weinberger, et al.
Published: (2019-02-01)

The Application of <sup>29</sup>Si NMR Spectroscopy to the Analysis of Calcium Silicate-Based Cement using Biodentine™ as an Example
by: Qiu Li, et al.
Published: (2019-05-01)

Assessing Heterogeneity of Osteolytic Lesions in Multiple Myeloma by 1H HR-MAS NMR Metabolomics
by: Laurette Tavel, et al.
Published: (2016-10-01)

Enzymatic modification of cassava starch (Corpoica M-Tai) around the pasting temperature
by: Jairo Salcedo-Mendoza, et al.
Published: (2018-01-01)

Solid-State NMR Studies of Solvent-Accessible Fragments of a Seven-Helical Transmembrane Protein Proteorhodopsin
by: Ward, Meaghan
Published: (2011)

Validation of the <sup>2</sup>H-SNIF NMR and IRMS Methods for Vinegar and Vinegar Analysis: An International Collaborative Study
by: Federica Camin, et al.
Published: (2020-06-01)

Unambiguous Assignment of the 1H- and 13C-NMR Spectra of Propafenone and a Thiophene Analogue
by: Wolfgang Holzer
Published: (2001-09-01)

Study of starch aging characteristics based on Terahertz technology
by: Tao Wang, et al.
Published: (2021-08-01)

Determination of Glyphosate in Dried Wheat by <sup>1</sup>H-NMR Spectroscopy
by: Elena Shumilina, et al.
Published: (2020-03-01)

Single-Crystal <sup>31</sup>P and <sup>7</sup>Li NMR of the Ionic Conductor LiH<sub>2</sub>PO<sub>4</sub>
by: Otto E. O. Zeman, et al.
Published: (2020-04-01)