Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene

Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene

The title compound, C15H17NO2, was synthesized from a mixture of α-himachalene (2-methylene-6,6,9-trimethylbicyclo[5.4.01,7]undec-8-ene) and β-himachalene (2,6,6,9-tetramethylbicyclo[5.4.01,7]undeca-1,8-diene), which were isolated from an oil of the Atlas cedar (Cedrus Atlantica). The naphthalene ri...

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Main Authors: Ahmed Benharref, Jamal Elkarroumi, Lahcen El Ammari, Mohamed Saadi, Moha Berraho
Format: Article
Language:English
Published: International Union of Crystallography 2015-09-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
essential oil of the Atlas cedar
nitro-naphthalene
C—H...O interaction
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989015014395
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spelling doaj-0d0eae8219a64b47af4bc78a2ce1d6d82020-11-24T23:31:39ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902015-09-01719o659o66010.1107/S2056989015014395is5409Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthaleneAhmed Benharref0Jamal Elkarroumi1Lahcen El Ammari2Mohamed Saadi3Moha Berraho4Laboratoire de Chimie des Substances Naturelles, "Unité Associé au CNRST (URAC16)", Faculté des Sciences Semlalia, BP 2390 Bd My Abdellah, 40000 Marrakech, MoroccoLaboratoire de Chimie des Substances Naturelles, "Unité Associé au CNRST (URAC16)", Faculté des Sciences Semlalia, BP 2390 Bd My Abdellah, 40000 Marrakech, MoroccoLaboratoire de Chimie du Solide, Appliquée, Faculté des Sciences, Université Mohammed V, Avenue Ibn Battouta, BP 1014, Rabat, MoroccoLaboratoire de Chimie du Solide, Appliquée, Faculté des Sciences, Université Mohammed V, Avenue Ibn Battouta, BP 1014, Rabat, MoroccoLaboratoire de Chimie des Substances Naturelles, "Unité Associé au CNRST (URAC16)", Faculté des Sciences Semlalia, BP 2390 Bd My Abdellah, 40000 Marrakech, MoroccoThe title compound, C15H17NO2, was synthesized from a mixture of α-himachalene (2-methylene-6,6,9-trimethylbicyclo[5.4.01,7]undec-8-ene) and β-himachalene (2,6,6,9-tetramethylbicyclo[5.4.01,7]undeca-1,8-diene), which were isolated from an oil of the Atlas cedar (Cedrus Atlantica). The naphthalene ring system makes dihedral angles of 68.6 (2) and 44.3 (2)°, respectively, with its attached isopropyl C/C/C plane and the nitro group. In the crystal, molecules held together by a C—H...O interaction, forming a chain along [-101].http://scripts.iucr.org/cgi-bin/paper?S2056989015014395crystal structureessential oil of the Atlas cedarnitro-naphthaleneC—H...O interaction
collection DOAJ
language English
format Article
sources DOAJ
author Ahmed Benharref
Jamal Elkarroumi
Lahcen El Ammari
Mohamed Saadi
Moha Berraho
spellingShingle Ahmed Benharref
Jamal Elkarroumi
Lahcen El Ammari
Mohamed Saadi
Moha Berraho
Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
Acta Crystallographica Section E: Crystallographic Communications
crystal structure
essential oil of the Atlas cedar
nitro-naphthalene
C—H...O interaction
author_facet Ahmed Benharref
Jamal Elkarroumi
Lahcen El Ammari
Mohamed Saadi
Moha Berraho
author_sort Ahmed Benharref
title Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
title_short Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
title_full Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
title_fullStr Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
title_full_unstemmed Crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
title_sort crystal structure of 1-isopropyl-4,7-dimethyl-3-nitronaphthalene
publisher International Union of Crystallography
series Acta Crystallographica Section E: Crystallographic Communications
issn 2056-9890
publishDate 2015-09-01
description The title compound, C15H17NO2, was synthesized from a mixture of α-himachalene (2-methylene-6,6,9-trimethylbicyclo[5.4.01,7]undec-8-ene) and β-himachalene (2,6,6,9-tetramethylbicyclo[5.4.01,7]undeca-1,8-diene), which were isolated from an oil of the Atlas cedar (Cedrus Atlantica). The naphthalene ring system makes dihedral angles of 68.6 (2) and 44.3 (2)°, respectively, with its attached isopropyl C/C/C plane and the nitro group. In the crystal, molecules held together by a C—H...O interaction, forming a chain along [-101].
topic crystal structure
essential oil of the Atlas cedar
nitro-naphthalene
C—H...O interaction
url http://scripts.iucr.org/cgi-bin/paper?S2056989015014395
work_keys_str_mv AT ahmedbenharref crystalstructureof1isopropyl47dimethyl3nitronaphthalene
AT jamalelkarroumi crystalstructureof1isopropyl47dimethyl3nitronaphthalene
AT lahcenelammari crystalstructureof1isopropyl47dimethyl3nitronaphthalene
AT mohamedsaadi crystalstructureof1isopropyl47dimethyl3nitronaphthalene
AT mohaberraho crystalstructureof1isopropyl47dimethyl3nitronaphthalene
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