Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate

Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate

The title salt, K+·C13H9O2−·H2O, was synthesized from 5-bromosalicylaldehyde and a phenylboronic acid derivative using the Suzuki–Miyaura cross-coupling reaction (Miyaura & Suzuki, 1979). In addition to the intermolecular interactions between the charged species, two O—H...O hydrogen bonds invol...

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Bibliographic Details
Main Authors: Ryoji Moriwaki, Tomoyuki Haraguchi, Takashiro Akitsu
Format: Article
Language:English
Published: International Union of Crystallography 2017-09-01
Series:IUCrData
Subjects:
crystal structure
cross coupling reactions
potassium cation
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2414314617013542
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spelling doaj-0c7101979d8249f8a338464de20aa0b22020-11-25T00:24:56ZengInternational Union of CrystallographyIUCrData2414-31462017-09-0129x17135410.1107/S2414314617013542zq4024Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrateRyoji Moriwaki0Tomoyuki Haraguchi1Takashiro Akitsu2Department of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, JapanDepartment of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, JapanDepartment of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, JapanThe title salt, K+·C13H9O2−·H2O, was synthesized from 5-bromosalicylaldehyde and a phenylboronic acid derivative using the Suzuki–Miyaura cross-coupling reaction (Miyaura & Suzuki, 1979). In addition to the intermolecular interactions between the charged species, two O—H...O hydrogen bonds involving the isolated water molecules further stabilize the crystal packing of the title salt leading to the formation of a three-dimensional framework structure.http://scripts.iucr.org/cgi-bin/paper?S2414314617013542crystal structurecross coupling reactionspotassium cation
collection DOAJ
language English
format Article
sources DOAJ
author Ryoji Moriwaki
Tomoyuki Haraguchi
Takashiro Akitsu
spellingShingle Ryoji Moriwaki
Tomoyuki Haraguchi
Takashiro Akitsu
Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
IUCrData
crystal structure
cross coupling reactions
potassium cation
author_facet Ryoji Moriwaki
Tomoyuki Haraguchi
Takashiro Akitsu
author_sort Ryoji Moriwaki
title Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
title_short Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
title_full Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
title_fullStr Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
title_full_unstemmed Potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
title_sort potassium 3-formyl-[1,1′-biphenyl]-4-olate monohydrate
publisher International Union of Crystallography
series IUCrData
issn 2414-3146
publishDate 2017-09-01
description The title salt, K+·C13H9O2−·H2O, was synthesized from 5-bromosalicylaldehyde and a phenylboronic acid derivative using the Suzuki–Miyaura cross-coupling reaction (Miyaura & Suzuki, 1979). In addition to the intermolecular interactions between the charged species, two O—H...O hydrogen bonds involving the isolated water molecules further stabilize the crystal packing of the title salt leading to the formation of a three-dimensional framework structure.
topic crystal structure
cross coupling reactions
potassium cation
url http://scripts.iucr.org/cgi-bin/paper?S2414314617013542
work_keys_str_mv AT ryojimoriwaki potassium3formyl11biphenyl4olatemonohydrate
AT tomoyukiharaguchi potassium3formyl11biphenyl4olatemonohydrate
AT takashiroakitsu potassium3formyl11biphenyl4olatemonohydrate
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