Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid

Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid

The molecular structures of (E)-non-2-enoic acid (C9) and (E)-dec-2-enoic acid (C10) are reported. The title compounds were crystallized by slow evaporation of ethanolic solutions at −30 °C. C9 crystallizes in the monoclinic space group P21/c and C10 in the triclinic space group P-1, each with 4 mol...

Full description

Bibliographic Details
Main Authors: Marcel Sonneck, Tim Peppel, Anke Spannenberg, Sebastian Wohlrab
Format: Article
Language:English
Published: MDPI AG 2015-10-01
Series:Crystals
Subjects:
X-ray crystal structure
hydrogen bond
dimer
unsaturated carboxylic acid
fatty acid
Online Access:http://www.mdpi.com/2073-4352/5/4/466
id doaj-0c486aed243c4087ba08bbe1bb8e97eb
record_format Article
spelling doaj-0c486aed243c4087ba08bbe1bb8e97eb2020-11-24T21:55:29ZengMDPI AGCrystals2073-43522015-10-015446647410.3390/cryst5040466cryst5040466Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic AcidMarcel Sonneck0Tim Peppel1Anke Spannenberg2Sebastian Wohlrab3Leibniz Institute for Catalysis at the University of Rostock (LIKAT), Albert-Einstein-Str. 29a, D-18059 Rostock, GermanyLeibniz Institute for Catalysis at the University of Rostock (LIKAT), Albert-Einstein-Str. 29a, D-18059 Rostock, GermanyLeibniz Institute for Catalysis at the University of Rostock (LIKAT), Albert-Einstein-Str. 29a, D-18059 Rostock, GermanyLeibniz Institute for Catalysis at the University of Rostock (LIKAT), Albert-Einstein-Str. 29a, D-18059 Rostock, GermanyThe molecular structures of (E)-non-2-enoic acid (C9) and (E)-dec-2-enoic acid (C10) are reported. The title compounds were crystallized by slow evaporation of ethanolic solutions at −30 °C. C9 crystallizes in the monoclinic space group P21/c and C10 in the triclinic space group P-1, each with 4 molecules in the unit cell. The unit cell parameters for C9 are: a = 10.6473(4) Å, b = 5.2855(2) Å, c = 17.0313(7) Å; β = 106.0985(10)° and V = 920.87(6) Å3. The unit cell parameters for C10 are: a = 4.1405(2) Å, b = 15.2839(6) Å, c = 17.7089(7) Å; α = 68.3291(11)°, β = 83.3850(13)°, γ = 85.0779(12)° and V = 1033.39(8) Å3.http://www.mdpi.com/2073-4352/5/4/466X-ray crystal structurehydrogen bonddimerunsaturated carboxylic acidfatty acid
collection DOAJ
language English
format Article
sources DOAJ
author Marcel Sonneck
Tim Peppel
Anke Spannenberg
Sebastian Wohlrab
spellingShingle Marcel Sonneck
Tim Peppel
Anke Spannenberg
Sebastian Wohlrab
Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid
Crystals
X-ray crystal structure
hydrogen bond
dimer
unsaturated carboxylic acid
fatty acid
author_facet Marcel Sonneck
Tim Peppel
Anke Spannenberg
Sebastian Wohlrab
author_sort Marcel Sonneck
title Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid
title_short Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid
title_full Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid
title_fullStr Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid
title_full_unstemmed Synthesis and Molecular Structures of (E)-non-2-enoic Acid and (E)-dec-2-enoic Acid
title_sort synthesis and molecular structures of (e)-non-2-enoic acid and (e)-dec-2-enoic acid
publisher MDPI AG
series Crystals
issn 2073-4352
publishDate 2015-10-01
description The molecular structures of (E)-non-2-enoic acid (C9) and (E)-dec-2-enoic acid (C10) are reported. The title compounds were crystallized by slow evaporation of ethanolic solutions at −30 °C. C9 crystallizes in the monoclinic space group P21/c and C10 in the triclinic space group P-1, each with 4 molecules in the unit cell. The unit cell parameters for C9 are: a = 10.6473(4) Å, b = 5.2855(2) Å, c = 17.0313(7) Å; β = 106.0985(10)° and V = 920.87(6) Å3. The unit cell parameters for C10 are: a = 4.1405(2) Å, b = 15.2839(6) Å, c = 17.7089(7) Å; α = 68.3291(11)°, β = 83.3850(13)°, γ = 85.0779(12)° and V = 1033.39(8) Å3.
topic X-ray crystal structure
hydrogen bond
dimer
unsaturated carboxylic acid
fatty acid
url http://www.mdpi.com/2073-4352/5/4/466
work_keys_str_mv AT marcelsonneck synthesisandmolecularstructuresofenon2enoicacidandedec2enoicacid
AT timpeppel synthesisandmolecularstructuresofenon2enoicacidandedec2enoicacid
AT ankespannenberg synthesisandmolecularstructuresofenon2enoicacidandedec2enoicacid
AT sebastianwohlrab synthesisandmolecularstructuresofenon2enoicacidandedec2enoicacid
_version_ 1725862412140150784

Similar Items