An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety
A new method has been developed for the synthesis of novel Schiff bases containg anthraquinone moiety using dodeca-Tungstosilicic acid/P2O5 under solvent free conditions at room temperature. The reaction was completed in 1-3 minutes with excellent yields. This method was found to be more efficie...
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Serbian Chemical Society
2013-01-01
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| Series: | Journal of the Serbian Chemical Society |
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| Online Access: | http://www.doiserbia.nb.rs/img/doi/0352-5139/2013/0352-51391200092F.pdf |
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doaj-0bacb9ac5adf4702bbeb2d8ab10f569d2020-11-24T22:50:27ZengSerbian Chemical Society Journal of the Serbian Chemical Society0352-51392013-01-0178447748210.2298/JSC120409092FAn efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moietyFareed GhulamVersiani Ali MuhammadAfza NighatFareed NaziaAli Irfan MuhammadKalhoro Ali MahboobA new method has been developed for the synthesis of novel Schiff bases containg anthraquinone moiety using dodeca-Tungstosilicic acid/P2O5 under solvent free conditions at room temperature. The reaction was completed in 1-3 minutes with excellent yields. This method was found to be more efficient, easy and hazardous free for the synthesis of azomethines. The development of these type of methadologies in synthetic chemistry may contribute to green chemistry. The structures of synthesized novel Schiff bases was elucidated using 1H-NMR, 13C-NMR, LCMS, FTIR and CHN analysis.http://www.doiserbia.nb.rs/img/doi/0352-5139/2013/0352-51391200092F.pdfazomethinedodeca-tungstosilicic acidP2O5anthraquinone |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Fareed Ghulam Versiani Ali Muhammad Afza Nighat Fareed Nazia Ali Irfan Muhammad Kalhoro Ali Mahboob |
| spellingShingle |
Fareed Ghulam Versiani Ali Muhammad Afza Nighat Fareed Nazia Ali Irfan Muhammad Kalhoro Ali Mahboob An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety Journal of the Serbian Chemical Society azomethine dodeca-tungstosilicic acid P2O5 anthraquinone |
| author_facet |
Fareed Ghulam Versiani Ali Muhammad Afza Nighat Fareed Nazia Ali Irfan Muhammad Kalhoro Ali Mahboob |
| author_sort |
Fareed Ghulam |
| title |
An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety |
| title_short |
An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety |
| title_full |
An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety |
| title_fullStr |
An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety |
| title_full_unstemmed |
An efficient synthesis and spectroscopic characterization of Schiff bases containing 9,10-anthracenedione moiety |
| title_sort |
efficient synthesis and spectroscopic characterization of schiff bases containing 9,10-anthracenedione moiety |
| publisher |
Serbian Chemical Society |
| series |
Journal of the Serbian Chemical Society |
| issn |
0352-5139 |
| publishDate |
2013-01-01 |
| description |
A new method has been developed for the synthesis of novel Schiff bases containg anthraquinone moiety using dodeca-Tungstosilicic acid/P2O5 under solvent free conditions at room temperature. The reaction was completed in 1-3 minutes with excellent yields. This method was found to be more efficient, easy and hazardous free for the synthesis of azomethines. The development of these type of methadologies in synthetic chemistry may contribute to green chemistry. The structures of synthesized novel Schiff bases was elucidated using 1H-NMR, 13C-NMR, LCMS, FTIR and CHN analysis. |
| topic |
azomethine dodeca-tungstosilicic acid P2O5 anthraquinone |
| url |
http://www.doiserbia.nb.rs/img/doi/0352-5139/2013/0352-51391200092F.pdf |
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