Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst

Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst

The clean, environmentally benign and effective synthesis of novel azo-linked 4-arylpyrimidin-2(1H)-one derivatives and 4,6-bisarylpyrimidin-2(1H)-ones via three-component reaction of various aldehydes or synthetized azo-linked aldehydes, urea, and acetophenone promoted by NiFe2O4@SiO2nPr@glucose am...

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Bibliographic Details
Main Authors: Mohammad Nikpassand, Elaheh hoseinnezhad
Format: Article
Language:English
Published: Elsevier 2020-12-01
Series:Arabian Journal of Chemistry
Subjects:
Pyrimidin-2(1H)-one
NiFe2O4@SiO2nPr@glucose amine
Urea
Nanoparticle
Green synthesis
Online Access:http://www.sciencedirect.com/science/article/pii/S1878535220304172
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spelling doaj-09aef2cee00a4f27805d3e1bf24be8412020-12-03T04:30:53ZengElsevierArabian Journal of Chemistry1878-53522020-12-01131289959004Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalystMohammad Nikpassand0Elaheh hoseinnezhad1Department of Chemistry, Rasht Branch, Islamic Azad University, Rasht, Iran; Corresponding author.Department of Chemistry, Ghadr Institute, Rasht, IranThe clean, environmentally benign and effective synthesis of novel azo-linked 4-arylpyrimidin-2(1H)-one derivatives and 4,6-bisarylpyrimidin-2(1H)-ones via three-component reaction of various aldehydes or synthetized azo-linked aldehydes, urea, and acetophenone promoted by NiFe2O4@SiO2nPr@glucose amine at room temperature (25 °C) was reported. NiFe2O4@SiO2nPr@glucose amine were synthesized and characterized by transmission electron microscope (TEM), fourier transform infrared spectroscopy (FT-IR), vibrating sample magnetometry (VSM), X-ray powder diffraction (XRD) and X-ray spectroscopy (EDX). These compounds were obtained in high yields and short reaction times. The catalyst could be easily recovered and reused for six cycles with almost consistent activity. The structures of the synthesized 4,6-bisarylpyrimidin-2(1H)-one compounds were confirmed by 1H NMR, 13C NMR and FTIR spectral data and elemental analyses.http://www.sciencedirect.com/science/article/pii/S1878535220304172Pyrimidin-2(1H)-oneNiFe2O4@SiO2nPr@glucose amineUreaNanoparticleGreen synthesis
collection DOAJ
language English
format Article
sources DOAJ
author Mohammad Nikpassand
Elaheh hoseinnezhad
spellingShingle Mohammad Nikpassand
Elaheh hoseinnezhad
Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst
Arabian Journal of Chemistry
Pyrimidin-2(1H)-one
NiFe2O4@SiO2nPr@glucose amine
Urea
Nanoparticle
Green synthesis
author_facet Mohammad Nikpassand
Elaheh hoseinnezhad
author_sort Mohammad Nikpassand
title Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst
title_short Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst
title_full Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst
title_fullStr Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst
title_full_unstemmed Green synthesis of 4,6-bisarylpyrimidin-2(1H)-ones and azo-linked 4-arylpyrimidin-2(1H)-ones using NiFe2O4@SiO2nPr@glucose amine as a mild nano catalyst
title_sort green synthesis of 4,6-bisarylpyrimidin-2(1h)-ones and azo-linked 4-arylpyrimidin-2(1h)-ones using nife2o4@sio2npr@glucose amine as a mild nano catalyst
publisher Elsevier
series Arabian Journal of Chemistry
issn 1878-5352
publishDate 2020-12-01
description The clean, environmentally benign and effective synthesis of novel azo-linked 4-arylpyrimidin-2(1H)-one derivatives and 4,6-bisarylpyrimidin-2(1H)-ones via three-component reaction of various aldehydes or synthetized azo-linked aldehydes, urea, and acetophenone promoted by NiFe2O4@SiO2nPr@glucose amine at room temperature (25 °C) was reported. NiFe2O4@SiO2nPr@glucose amine were synthesized and characterized by transmission electron microscope (TEM), fourier transform infrared spectroscopy (FT-IR), vibrating sample magnetometry (VSM), X-ray powder diffraction (XRD) and X-ray spectroscopy (EDX). These compounds were obtained in high yields and short reaction times. The catalyst could be easily recovered and reused for six cycles with almost consistent activity. The structures of the synthesized 4,6-bisarylpyrimidin-2(1H)-one compounds were confirmed by 1H NMR, 13C NMR and FTIR spectral data and elemental analyses.
topic Pyrimidin-2(1H)-one
NiFe2O4@SiO2nPr@glucose amine
Urea
Nanoparticle
Green synthesis
url http://www.sciencedirect.com/science/article/pii/S1878535220304172
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