4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

The title Schiff base compound, C22H24IN3O2, adopts an E configuration about the central C=N bond. The pyrazolone ring makes a dihedral angle of 49.68 (10)° with its attached phenyl ring. The phenolate plane makes dihedral angles of 16.78 (9) and 50.54&am...

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Main Authors: Hoong-Kun Fun, Madhukar Hemamalini, Abdullah M. Asiri, Salman A. Khan
Format: Article
Language:English
Published: International Union of Crystallography 2010-07-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810020374
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spelling doaj-07762bf0b8414c52b52ca60d31ae31ee2020-11-25T02:14:00ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-07-01667o1588o158910.1107/S16005368100203744-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-oneHoong-Kun FunMadhukar HemamaliniAbdullah M. AsiriSalman A. KhanThe title Schiff base compound, C22H24IN3O2, adopts an E configuration about the central C=N bond. The pyrazolone ring makes a dihedral angle of 49.68 (10)° with its attached phenyl ring. The phenolate plane makes dihedral angles of 16.78 (9) and 50.54 (9)°, respectively, with the pyrazolone ring and the terminal phenyl ring. An intramolecular C—H...O hydrogen bond generates an S(6) ring motif. In the crystal structure, an intermolecular C—H...O hydrogen bond is also observed. http://scripts.iucr.org/cgi-bin/paper?S1600536810020374
collection DOAJ
language English
format Article
sources DOAJ
author Hoong-Kun Fun
Madhukar Hemamalini
Abdullah M. Asiri
Salman A. Khan
spellingShingle Hoong-Kun Fun
Madhukar Hemamalini
Abdullah M. Asiri
Salman A. Khan
4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
Acta Crystallographica Section E
author_facet Hoong-Kun Fun
Madhukar Hemamalini
Abdullah M. Asiri
Salman A. Khan
author_sort Hoong-Kun Fun
title 4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
title_short 4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
title_full 4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
title_fullStr 4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
title_full_unstemmed 4-{(E)-[2-(4-Iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
title_sort 4-{(e)-[2-(4-iodobutoxy)benzylidene]amino}-1,5-dimethyl-2-phenyl-1h-pyrazol-3(2h)-one
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2010-07-01
description The title Schiff base compound, C22H24IN3O2, adopts an E configuration about the central C=N bond. The pyrazolone ring makes a dihedral angle of 49.68 (10)° with its attached phenyl ring. The phenolate plane makes dihedral angles of 16.78 (9) and 50.54 (9)°, respectively, with the pyrazolone ring and the terminal phenyl ring. An intramolecular C—H...O hydrogen bond generates an S(6) ring motif. In the crystal structure, an intermolecular C—H...O hydrogen bond is also observed.
url http://scripts.iucr.org/cgi-bin/paper?S1600536810020374
work_keys_str_mv AT hoongkunfun 4e24iodobutoxybenzylideneamino15dimethyl2phenyl1hpyrazol32hone
AT madhukarhemamalini 4e24iodobutoxybenzylideneamino15dimethyl2phenyl1hpyrazol32hone
AT abdullahmasiri 4e24iodobutoxybenzylideneamino15dimethyl2phenyl1hpyrazol32hone
AT salmanakhan 4e24iodobutoxybenzylideneamino15dimethyl2phenyl1hpyrazol32hone
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