3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione

3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione

The title compound, C28H30N2OS2, was obtained by thionation of 3′,6′-bis(diethylamino)-3H-spiro[isobenzofuran-1,9′-xanthene]-3-one with 2,4-bis(p-methoxyphenyl)-1,3-dithiadiphosphetane disulfide (Lawesson's reagent). The planes of the two benzene rings of the xanth...

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Main Authors: Bing-Yuan Su, Xin-Qi Zhan, Jian-Nan Guo, Yue-Feng Zhou, Hong Zheng
Format: Article
Language:English
Published: International Union of Crystallography 2008-11-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536808031218
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spelling doaj-020a4d1a7e3e4a74922d87339425dcb92020-11-24T21:26:39ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-11-016411o2068o206810.1107/S16005368080312183′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thioneBing-Yuan SuXin-Qi ZhanJian-Nan GuoYue-Feng ZhouHong ZhengThe title compound, C28H30N2OS2, was obtained by thionation of 3′,6′-bis(diethylamino)-3H-spiro[isobenzofuran-1,9′-xanthene]-3-one with 2,4-bis(p-methoxyphenyl)-1,3-dithiadiphosphetane disulfide (Lawesson's reagent). The planes of the two benzene rings of the xanthene system are inclined at a dihedral angle of 17.4 (1)°, and the plane of the dithiophthalide group and the planes through the two benzene rings of the xanthene system make dihedral angles of 80.2 (1) and 82.8 (1)°, respectively.http://scripts.iucr.org/cgi-bin/paper?S1600536808031218
collection DOAJ
language English
format Article
sources DOAJ
author Bing-Yuan Su
Xin-Qi Zhan
Jian-Nan Guo
Yue-Feng Zhou
Hong Zheng
spellingShingle Bing-Yuan Su
Xin-Qi Zhan
Jian-Nan Guo
Yue-Feng Zhou
Hong Zheng
3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
Acta Crystallographica Section E
author_facet Bing-Yuan Su
Xin-Qi Zhan
Jian-Nan Guo
Yue-Feng Zhou
Hong Zheng
author_sort Bing-Yuan Su
title 3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
title_short 3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
title_full 3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
title_fullStr 3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
title_full_unstemmed 3′,6′-Bis(diethylamino)-3H-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
title_sort 3′,6′-bis(diethylamino)-3h-spiro[2-benzothiophene-1,9′-xanthene]-3-thione
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2008-11-01
description The title compound, C28H30N2OS2, was obtained by thionation of 3′,6′-bis(diethylamino)-3H-spiro[isobenzofuran-1,9′-xanthene]-3-one with 2,4-bis(p-methoxyphenyl)-1,3-dithiadiphosphetane disulfide (Lawesson's reagent). The planes of the two benzene rings of the xanthene system are inclined at a dihedral angle of 17.4 (1)°, and the plane of the dithiophthalide group and the planes through the two benzene rings of the xanthene system make dihedral angles of 80.2 (1) and 82.8 (1)°, respectively.
url http://scripts.iucr.org/cgi-bin/paper?S1600536808031218
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AT xinqizhan 3824268242bisdiethylamino3hspiro2benzothiophene198242xanthene3thione
AT jiannanguo 3824268242bisdiethylamino3hspiro2benzothiophene198242xanthene3thione
AT yuefengzhou 3824268242bisdiethylamino3hspiro2benzothiophene198242xanthene3thione
AT hongzheng 3824268242bisdiethylamino3hspiro2benzothiophene198242xanthene3thione
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